Chemical Industry and Engineering Progress ›› 2019, Vol. 38 ›› Issue (07): 3227-3242.DOI: 10.16085/j.issn.1000-6613.2018-1919
• Materials science and technology • Previous Articles Next Articles
Ying PENG(),Xiaowen ZHANG(),Mi LI,Yu ZHANG,Xiaoyan WU
Received:
2018-09-25
Online:
2019-07-05
Published:
2019-07-05
Contact:
Xiaowen ZHANG
通讯作者:
张晓文
作者简介:
彭莹(1987—),女,博士研究生,研究方向为新型材料的合成及在环境领域的应用。E-mail:<email>pengying415@163.com</email>。
基金资助:
CLC Number:
Ying PENG, Xiaowen ZHANG, Mi LI, Yu ZHANG, Xiaoyan WU. Application of metal-organic frameworks in adsorption and separation of uranium from water[J]. Chemical Industry and Engineering Progress, 2019, 38(07): 3227-3242.
彭莹, 张晓文, 李密, 张宇, 吴晓燕. 金属有机框架材料吸附分离水中铀的应用[J]. 化工进展, 2019, 38(07): 3227-3242.
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吸附剂 | 比表面积 /m2·g-1 | 最佳pH | 固液比 /g·L-1 | q max /mg·g-1 | 符合的动力学模型 | 符合的热力学方程 | 吸附机理 | 参考文献 | |||
---|---|---|---|---|---|---|---|---|---|---|---|
UiO-68-DPPU | 1350 | 2.5 | 1 | 217 | — | Langmuir | DFT计算得出DPPU与UO2 2+的吸附原理符合2:1的结合模式 | [ | |||
MOF-76 | — | 3.0 | 0.4 | 298 | — | Langmuir | — | [ | |||
HKUST-1 | 6 | 0.6 | 787.4 | 准二级 | Langmuir | 通过热力学参数ΔG、ΔH、ΔS推测吸附过程是自发吸热的过程 | [ | ||||
MIL-101(Cr)-ED | 517 | 4.5 | 0.5 | 200(exp, c 0=100mg·L-1) | — | — | X射线吸收光谱(XANES+EXAFS)研究了铀与氨基的结合模式和ED嫁接量的影响 | [ | |||
MIL-101 | 3065 | 5 | 0.4 | 20(exp) | 准二级 | Langmuir | FTIR和EXAFS联合分析得出MIL-101-NH2上的NH2由于苯环的空间位阻作用而影响了U-N的结合 | [ | |||
MIL-101-NH2 | 1645 | 90(exp) | |||||||||
MIL-101-DETA | 1074 | 350(exp) | |||||||||
MIL-101-ED | 753 | 200(exp) | |||||||||
Zn(HBTC)(L)·(H2O)2 | — | 2 | — | 0.53① | 准二级 | Langmuir | IR光谱分析推测吸附作用主要是由于MOF材料1D通道上独立的羧基与UO2 2+的U-O键合作用 | [ | |||
MIL-101-COOH | 890.5 | 7 | — | 314 | 准二级 | Langmuir | MDS(分子动力学模拟)和DFT(密度泛函理论计算)联合从分子水平分析了MOFs与U的结合 | [ | |||
Coumarin-modified Zn-MOF-74 | — | 4 | 1 | 360(exp, c 0=400mg·L-1) | 准二级 | — | — | [ | |||
UiO-66 | 1382 | 109.9 | 准二级 | Langmuir | 简单推测NH2并没有提高UiO-66吸附能力的原因是苯环上氨基的低活性、比表面积的降低和NH2之间氢键的形成 | [ | |||||
UiO-66-NH2 | 1050 | 5.5 | 0.4 | 114.9 | |||||||
HKUST-1@H3PW12O40 | 467 | 6 | 0.2 | 14.58 | 准二级 | Langmuir | 通过热力学参数ΔG,ΔH,ΔS推测吸附过程是自发吸热的过程 | [ | |||
UiO-66-AO | 711 | — | — | 2.68② | 准二级 | — | EXAFS分析得出偕胺肟能够与U(Ⅵ)进行螯合,形成六角形双锥体配位几何体 | [ | |||
MIL-53(Al)-AO | — | 5.5 | 0.4 | 454.54 | 准二级 | Freundlich | — | [ | |||
CMPO@MIL-101(Cr) | 1014 | — | — | — | — | — | 该篇文献主要是研究材料很好的选择性和可重复利用性,批实验和机理分析少 | [ | |||
MIL-101-Ship | 2365 | 4 | 1 | 27.99 | 准二级 | Langmuir | — | [ | |||
Fe3O4@ZIF-8 | 1137 | 3 | — | 523.5(exp) | 准二级 | Langmuir | — | [ | |||
Fe3O4@AMCA-MIL53(Al) | 197.8 | 5.5 | 0.8 | 227.3 | 准二级 | Langmuir | 通过热力学参数ΔG、ΔH、ΔS推测吸附过程是自发吸热的过程 | [ | |||
GO–COOH/UiO-66 | 767.12 | 8 | 0.5 | 998(exp, c 0=502.2mg·L-1) | 准二级 | Langmuir | FTIR光谱法、X射线光电子能谱(XPS)和XRD联合分析得出COOH和铀主要是螯合作用,还有一点离子交换作用 | [ | |||
Co-SLUG-35 | — | 9 | — | 1.03③ | 准二级 | Langmuir | FTIR、SEM、XPS分析得出MOFs对铀的吸附机理是阴离子交换 | [ | |||
MIL-100(Al) | — | 5 | — | 110(exp, c e=10000mg·L-1) | 准二级 | Freundlich | — | [ | |||
SZ-1 | 10.2 | — | — | — | — | — | XAS(XANES+EXAFS)、XPS光谱和MDS模拟表明,UO2 2 +和SZ-2之间的强静电相互作用有效地将UO2 2+驱动到SZ-2的骨架中,而更紧密的氢键网络的形成导致UO2 2+被充分捕获 | [ | |||
SZ-2 | 225 | 4.5 | — | 58.18 | — | Langmuir | |||||
SZ-3 | 594 | 4.5 | 58.18 | — | Langmuir |
吸附剂 | 比表面积 /m2·g-1 | 最佳pH | 固液比 /g·L-1 | q max /mg·g-1 | 符合的动力学模型 | 符合的热力学方程 | 吸附机理 | 参考文献 | |||
---|---|---|---|---|---|---|---|---|---|---|---|
UiO-68-DPPU | 1350 | 2.5 | 1 | 217 | — | Langmuir | DFT计算得出DPPU与UO2 2+的吸附原理符合2:1的结合模式 | [ | |||
MOF-76 | — | 3.0 | 0.4 | 298 | — | Langmuir | — | [ | |||
HKUST-1 | 6 | 0.6 | 787.4 | 准二级 | Langmuir | 通过热力学参数ΔG、ΔH、ΔS推测吸附过程是自发吸热的过程 | [ | ||||
MIL-101(Cr)-ED | 517 | 4.5 | 0.5 | 200(exp, c 0=100mg·L-1) | — | — | X射线吸收光谱(XANES+EXAFS)研究了铀与氨基的结合模式和ED嫁接量的影响 | [ | |||
MIL-101 | 3065 | 5 | 0.4 | 20(exp) | 准二级 | Langmuir | FTIR和EXAFS联合分析得出MIL-101-NH2上的NH2由于苯环的空间位阻作用而影响了U-N的结合 | [ | |||
MIL-101-NH2 | 1645 | 90(exp) | |||||||||
MIL-101-DETA | 1074 | 350(exp) | |||||||||
MIL-101-ED | 753 | 200(exp) | |||||||||
Zn(HBTC)(L)·(H2O)2 | — | 2 | — | 0.53① | 准二级 | Langmuir | IR光谱分析推测吸附作用主要是由于MOF材料1D通道上独立的羧基与UO2 2+的U-O键合作用 | [ | |||
MIL-101-COOH | 890.5 | 7 | — | 314 | 准二级 | Langmuir | MDS(分子动力学模拟)和DFT(密度泛函理论计算)联合从分子水平分析了MOFs与U的结合 | [ | |||
Coumarin-modified Zn-MOF-74 | — | 4 | 1 | 360(exp, c 0=400mg·L-1) | 准二级 | — | — | [ | |||
UiO-66 | 1382 | 109.9 | 准二级 | Langmuir | 简单推测NH2并没有提高UiO-66吸附能力的原因是苯环上氨基的低活性、比表面积的降低和NH2之间氢键的形成 | [ | |||||
UiO-66-NH2 | 1050 | 5.5 | 0.4 | 114.9 | |||||||
HKUST-1@H3PW12O40 | 467 | 6 | 0.2 | 14.58 | 准二级 | Langmuir | 通过热力学参数ΔG,ΔH,ΔS推测吸附过程是自发吸热的过程 | [ | |||
UiO-66-AO | 711 | — | — | 2.68② | 准二级 | — | EXAFS分析得出偕胺肟能够与U(Ⅵ)进行螯合,形成六角形双锥体配位几何体 | [ | |||
MIL-53(Al)-AO | — | 5.5 | 0.4 | 454.54 | 准二级 | Freundlich | — | [ | |||
CMPO@MIL-101(Cr) | 1014 | — | — | — | — | — | 该篇文献主要是研究材料很好的选择性和可重复利用性,批实验和机理分析少 | [ | |||
MIL-101-Ship | 2365 | 4 | 1 | 27.99 | 准二级 | Langmuir | — | [ | |||
Fe3O4@ZIF-8 | 1137 | 3 | — | 523.5(exp) | 准二级 | Langmuir | — | [ | |||
Fe3O4@AMCA-MIL53(Al) | 197.8 | 5.5 | 0.8 | 227.3 | 准二级 | Langmuir | 通过热力学参数ΔG、ΔH、ΔS推测吸附过程是自发吸热的过程 | [ | |||
GO–COOH/UiO-66 | 767.12 | 8 | 0.5 | 998(exp, c 0=502.2mg·L-1) | 准二级 | Langmuir | FTIR光谱法、X射线光电子能谱(XPS)和XRD联合分析得出COOH和铀主要是螯合作用,还有一点离子交换作用 | [ | |||
Co-SLUG-35 | — | 9 | — | 1.03③ | 准二级 | Langmuir | FTIR、SEM、XPS分析得出MOFs对铀的吸附机理是阴离子交换 | [ | |||
MIL-100(Al) | — | 5 | — | 110(exp, c e=10000mg·L-1) | 准二级 | Freundlich | — | [ | |||
SZ-1 | 10.2 | — | — | — | — | — | XAS(XANES+EXAFS)、XPS光谱和MDS模拟表明,UO2 2 +和SZ-2之间的强静电相互作用有效地将UO2 2+驱动到SZ-2的骨架中,而更紧密的氢键网络的形成导致UO2 2+被充分捕获 | [ | |||
SZ-2 | 225 | 4.5 | — | 58.18 | — | Langmuir | |||||
SZ-3 | 594 | 4.5 | 58.18 | — | Langmuir |
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