Chemical Industry and Engineering Progress ›› 2021, Vol. 40 ›› Issue (8): 4371-4380.DOI: 10.16085/j.issn.1000-6613.2020-1901
• Materials science and technology • Previous Articles Next Articles
Synthesis and utilization of Pt and Pd nanoparticle-decorated MoS2 nanocomposites for fabrication of electrochemical biosensor
ZHOU Liya1(
), ZHOU Xitong1, ZHAO Congli2, JIANG Yanjun1, MA Li1(), He Ying1
- 1.School of Chemical Engineering and Technology, Hebei University of Technology, Tianjin 300130, China
2.School of Health Science and Engineering, Tianjin University of Traditional Chinese Medicine, Tianjin 301617, China
-
Received:2020-09-17Online:2021-08-12Published:2021-08-05 -
Contact:MA Li
基于铂、钯负载的MoS2纳米片构建生物传感器及应用
周丽亚1(), 周栖桐1, 赵聪俐2, 姜艳军1, 马丽1(), 贺莹1
- 1.河北工业大学化工学院，天津 300130
2.天津中医药大学健康科学与工程学院，天津 301617
-
通讯作者:马丽 -
作者简介:周丽亚（1976—），女，博士，教授，研究方向为生物传感器和酶分子定向改造。E-mail：liyazhou@hebut.edu.cn 。 -
基金资助:国家自然科学基金(21576068);河北省自然科学基金(B2017202056)
CLC Number:
Cite this article
ZHOU Liya, ZHOU Xitong, ZHAO Congli, JIANG Yanjun, MA Li, He Ying. Synthesis and utilization of Pt and Pd nanoparticle-decorated MoS2 nanocomposites for fabrication of electrochemical biosensor[J]. Chemical Industry and Engineering Progress, 2021, 40(8): 4371-4380.
周丽亚, 周栖桐, 赵聪俐, 姜艳军, 马丽, 贺莹. 基于铂、钯负载的MoS2纳米片构建生物传感器及应用[J]. 化工进展, 2021, 40(8): 4371-4380.
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| 构建电极 | 检测范围/mol·L-1 | 检测限/mol·L-1 | 参考文献 |
|---|---|---|---|
| AChE/PEDOT-MWCNTs/FTO | 1×10-11~1×10-9 | 1×10-11 | ［ |
| AChE-CS/Pd-Cu NWs/GCE | 1.5×10-13~3×10-9 和1.5×10-9~9×10-9 | 4.5×10-9 | ［ |
| AChE-Ag | 1×10-11~1×10-8 | 4.0 ×10-12 | ［ |
| AChE-CS/3DG-CuO NFs/GCE | 3×10-12~4.7×10-8 | 9.2×10-13 | ［ |
| AChE-CS/Pd@Au NRs/GCE | 3.6×10-12~1×10-7 | 3.6×10-12 | ［ |
| AChE/AuNPs/DAR/P-ABSA/GCE | 1×10-8~1×10-12 | 5.12×10-13 | ［ |
| AChE/CS-Ti3C2Tx/GCE | 1×10-14~1×10-8 | 0.3×10-14 | ［ |
| AChE/MPtPdN/GCE | 1×10-12~4.7×10-6 | 2.6×10-13 | ［ |
| AChE/ Pt-Pd/MoS2/GCE | 1×10-14~1×10-5 | 5.23×10-15 | 本文 |
| 构建电极 | 检测范围/mol·L-1 | 检测限/mol·L-1 | 参考文献 |
|---|---|---|---|
| AChE/PEDOT-MWCNTs/FTO | 1×10-11~1×10-9 | 1×10-11 | ［ |
| AChE-CS/Pd-Cu NWs/GCE | 1.5×10-13~3×10-9 和1.5×10-9~9×10-9 | 4.5×10-9 | ［ |
| AChE-Ag | 1×10-11~1×10-8 | 4.0 ×10-12 | ［ |
| AChE-CS/3DG-CuO NFs/GCE | 3×10-12~4.7×10-8 | 9.2×10-13 | ［ |
| AChE-CS/Pd@Au NRs/GCE | 3.6×10-12~1×10-7 | 3.6×10-12 | ［ |
| AChE/AuNPs/DAR/P-ABSA/GCE | 1×10-8~1×10-12 | 5.12×10-13 | ［ |
| AChE/CS-Ti3C2Tx/GCE | 1×10-14~1×10-8 | 0.3×10-14 | ［ |
| AChE/MPtPdN/GCE | 1×10-12~4.7×10-6 | 2.6×10-13 | ［ |
| AChE/ Pt-Pd/MoS2/GCE | 1×10-14~1×10-5 | 5.23×10-15 | 本文 |
| 样品 | 加入量 /mol·L-1 | 检出量 /mol·L-1 | 回收率 /% | 相对标准偏差 /% |
|---|---|---|---|---|
| 马拉硫磷 | ||||
| 1# | 1.00×10-9 | 0.932×10-9 | 93.2 | 2.1 |
| 2# | 1.00×10-10 | 0.943×10-10 | 94.3 | 1.9 |
| 3# | 1.00×10-11 | 0.999×10-11 | 99.9 | 4.1 |
| 甲基对硫磷 | ||||
| 1# | 1.00×10-9 | 0.914×10-9 | 91.4 | 4.5 |
| 2# | 1.00×10-10 | 0.962×10-10 | 96.2 | 3.3 |
| 3# | 1.00×10-11 | 1.03×10-11 | 103 | 4.2 |
| 样品 | 加入量 /mol·L-1 | 检出量 /mol·L-1 | 回收率 /% | 相对标准偏差 /% |
|---|---|---|---|---|
| 马拉硫磷 | ||||
| 1# | 1.00×10-9 | 0.932×10-9 | 93.2 | 2.1 |
| 2# | 1.00×10-10 | 0.943×10-10 | 94.3 | 1.9 |
| 3# | 1.00×10-11 | 0.999×10-11 | 99.9 | 4.1 |
| 甲基对硫磷 | ||||
| 1# | 1.00×10-9 | 0.914×10-9 | 91.4 | 4.5 |
| 2# | 1.00×10-10 | 0.962×10-10 | 96.2 | 3.3 |
| 3# | 1.00×10-11 | 1.03×10-11 | 103 | 4.2 |
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