Chemical Industry and Engineering Progress ›› 2023, Vol. 42 ›› Issue (10): 5299-5309.DOI: 10.16085/j.issn.1000-6613.2022-2180
• Materials science and technology • Previous Articles Next Articles
SONG Yali1(), LI Ziyan1, YANG Cairong1, HUANG Long2, ZHANG Hongzhong1()
Received:
2022-11-23
Revised:
2023-06-04
Online:
2023-11-11
Published:
2023-10-15
Contact:
ZHANG Hongzhong
宋亚丽1(), 李紫燕1, 杨彩荣1, 黄龙2, 张宏忠1()
通讯作者:
张宏忠
作者简介:
宋亚丽(1988—),女,博士,讲师,主要研究方向为光催化技术在水体修复中的应用。E-mail:songyl@zzuli.edu.cn。
基金资助:
CLC Number:
SONG Yali, LI Ziyan, YANG Cairong, HUANG Long, ZHANG Hongzhong. Research progress of non-metallic element doped graphitic carbon nitride photocatalytic materials[J]. Chemical Industry and Engineering Progress, 2023, 42(10): 5299-5309.
宋亚丽, 李紫燕, 杨彩荣, 黄龙, 张宏忠. 非金属元素掺杂石墨相氮化碳光催化材料的研究进展[J]. 化工进展, 2023, 42(10): 5299-5309.
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序号 | 前体物质 | 掺杂元素 | 取代位点 | 带隙能量(掺杂后/未掺杂)/eV | 光催化活性评价指标 | 去除率或产氢率或产氨率(掺杂后/未掺杂) |
---|---|---|---|---|---|---|
1 | 尿素+咪唑 | N | C1 | 2.26/2.72 | 罗丹明B去除率 | 93.5%/47%(提高2倍)[ |
2 | 双氰胺+二甲基甲酰胺 | C | N3 | 2.66/2.72 | 产氢率 | 8.88μmol·h-1/1.70μmol·h-1(提高5.2倍)[ |
3 | 氰胺+硫脲 | S | N2 | — | 产氢率 | 12.16μmol·h-1/2.03μmol·h-1(提高6.0倍)[ |
4 | 尿素+1-丁基-3-甲基咪唑六氟磷酸盐 | P | — | 2.31/2.70 | 四环素去除率 | 85%/40%(提高2.1倍)[ |
5 | 尿素 | O | N2 | 2.78/2.86 | 磺胺嘧啶去除率 | 72.64%/38.84%(提高1.8倍)[ |
6 | 尿素 | O | N1 | — | 罗丹明B去除率 | 99%/33%(提高3倍)[ |
7 | 硼酸+尿素 | B | — | 2.44/2.7 | 亚甲基蓝去除率 | 86%/11%(提高7.8倍)[ |
8 | 尿素+卤化铵 | F | N3 | 2.55/2.78 | 全氟辛酸去除率 | 74.3%/57.1%(提高1.3倍)[ |
9 | 三聚氯氰+双氰胺+乙腈 | Cl | N2 | 1.78/1.82 | 罗丹明B去除率 | 99.6%/16.8%(提高5.9倍)[ |
10 | 三聚氰胺+铵盐 | Br | 层间N | 2.75/2.78 | 土霉素去除率 | 75%/30%(提高2.5倍)[ |
11 | 双氰胺+碘酸钾 | I | N2 | 2.68/2.76 | 产氨率 | 200.8mg·L-1·g-1/71.9 mg·L-1·g-1(提高2.8倍)[ |
序号 | 前体物质 | 掺杂元素 | 取代位点 | 带隙能量(掺杂后/未掺杂)/eV | 光催化活性评价指标 | 去除率或产氢率或产氨率(掺杂后/未掺杂) |
---|---|---|---|---|---|---|
1 | 尿素+咪唑 | N | C1 | 2.26/2.72 | 罗丹明B去除率 | 93.5%/47%(提高2倍)[ |
2 | 双氰胺+二甲基甲酰胺 | C | N3 | 2.66/2.72 | 产氢率 | 8.88μmol·h-1/1.70μmol·h-1(提高5.2倍)[ |
3 | 氰胺+硫脲 | S | N2 | — | 产氢率 | 12.16μmol·h-1/2.03μmol·h-1(提高6.0倍)[ |
4 | 尿素+1-丁基-3-甲基咪唑六氟磷酸盐 | P | — | 2.31/2.70 | 四环素去除率 | 85%/40%(提高2.1倍)[ |
5 | 尿素 | O | N2 | 2.78/2.86 | 磺胺嘧啶去除率 | 72.64%/38.84%(提高1.8倍)[ |
6 | 尿素 | O | N1 | — | 罗丹明B去除率 | 99%/33%(提高3倍)[ |
7 | 硼酸+尿素 | B | — | 2.44/2.7 | 亚甲基蓝去除率 | 86%/11%(提高7.8倍)[ |
8 | 尿素+卤化铵 | F | N3 | 2.55/2.78 | 全氟辛酸去除率 | 74.3%/57.1%(提高1.3倍)[ |
9 | 三聚氯氰+双氰胺+乙腈 | Cl | N2 | 1.78/1.82 | 罗丹明B去除率 | 99.6%/16.8%(提高5.9倍)[ |
10 | 三聚氰胺+铵盐 | Br | 层间N | 2.75/2.78 | 土霉素去除率 | 75%/30%(提高2.5倍)[ |
11 | 双氰胺+碘酸钾 | I | N2 | 2.68/2.76 | 产氨率 | 200.8mg·L-1·g-1/71.9 mg·L-1·g-1(提高2.8倍)[ |
序号 | 前驱体物质 | 掺杂元素 | 取代位置 | 催化活性评价 指标 | 去除率或产氢率 | 参考文献 | ||
---|---|---|---|---|---|---|---|---|
g-C3N4 | 单元素掺杂 | 多元素共掺杂 | ||||||
1 | 三聚氰胺+六氯三磷腈+硫 | P、S | P取代C1位点 S取代N2位点 | 甲基蓝去除率 | 58% | 69%(P掺杂) 55%(S掺杂) | 完全降解 | [ |
2 | 双氰胺+谷胱甘肽 | C、O | C取代N1位点 O取代N2位点 | 产氢率 | 0.23mmol·h-1·g-1 | — | 18.38mmol·h-1·g-1 | [ |
3 | 植酸+三聚氰胺 | P、C | — | 产氢率 | 153.9μmol·g-1·h-1 | — | 1493.3μmol·g-1·h-1 | [ |
4 | 三聚氰胺+乙醇 | C、O | C取代N3位点 O取代N2位点 | 产氢率 | 93μmol·g-1·h-1 | — | 395μmol·g-1·h-1 | [ |
5 | 双氰胺+尿素+ 四氟硼酸乙基吡啶 | B、F | — | 产氢率 | 36μmol·h-1 | — | 343.5μmol·h-1 | [ |
6 | 三聚氰胺+H2O2+三硫氰酸 | S、O | S取代N2位点 O取代N2位点 | 罗丹明B去除率 | 20 % | 48%(S掺杂) | 75% | [ |
7 | 三聚氰胺+磷酸铵+氯化铵 | P、Cl | P取代C1位点 Cl占据间隙位点 | 罗丹明B去除率 | 60% | 66.02%(P掺杂) 97.91%(Cl掺杂) | 99.62% | [ |
8 | 硫脲+磷酸氢二胺 | S、P | — | 罗丹明B去除率 | 15% | 23%(S掺杂) | 66% | [ |
9 | 双氰胺+硝酸+磷酸氢二铵 | P、O | — | 罗丹明B去除率 | 13% | 37%(O掺杂) | 95% | [ |
10 | 六氯环三磷腈+硫脲 | P、S | — | 四环素去除率 | 32.95% | 43.48%(P掺杂) 73.50%(S掺杂) | 85.85% | [ |
11 | 三聚氰胺+硫脲+ 磷酸氢二铵 | P、S和O | P取代C1位点 O取代N2位点 S占据间隙位点 | 产氢率 | 467.33μmol·g-1·h-1 | 574μmol·g-1·h-1(S掺杂) 1141μmol·g-1·h-1(P掺杂) | 2479μmol·g-1·h-1 | [ |
序号 | 前驱体物质 | 掺杂元素 | 取代位置 | 催化活性评价 指标 | 去除率或产氢率 | 参考文献 | ||
---|---|---|---|---|---|---|---|---|
g-C3N4 | 单元素掺杂 | 多元素共掺杂 | ||||||
1 | 三聚氰胺+六氯三磷腈+硫 | P、S | P取代C1位点 S取代N2位点 | 甲基蓝去除率 | 58% | 69%(P掺杂) 55%(S掺杂) | 完全降解 | [ |
2 | 双氰胺+谷胱甘肽 | C、O | C取代N1位点 O取代N2位点 | 产氢率 | 0.23mmol·h-1·g-1 | — | 18.38mmol·h-1·g-1 | [ |
3 | 植酸+三聚氰胺 | P、C | — | 产氢率 | 153.9μmol·g-1·h-1 | — | 1493.3μmol·g-1·h-1 | [ |
4 | 三聚氰胺+乙醇 | C、O | C取代N3位点 O取代N2位点 | 产氢率 | 93μmol·g-1·h-1 | — | 395μmol·g-1·h-1 | [ |
5 | 双氰胺+尿素+ 四氟硼酸乙基吡啶 | B、F | — | 产氢率 | 36μmol·h-1 | — | 343.5μmol·h-1 | [ |
6 | 三聚氰胺+H2O2+三硫氰酸 | S、O | S取代N2位点 O取代N2位点 | 罗丹明B去除率 | 20 % | 48%(S掺杂) | 75% | [ |
7 | 三聚氰胺+磷酸铵+氯化铵 | P、Cl | P取代C1位点 Cl占据间隙位点 | 罗丹明B去除率 | 60% | 66.02%(P掺杂) 97.91%(Cl掺杂) | 99.62% | [ |
8 | 硫脲+磷酸氢二胺 | S、P | — | 罗丹明B去除率 | 15% | 23%(S掺杂) | 66% | [ |
9 | 双氰胺+硝酸+磷酸氢二铵 | P、O | — | 罗丹明B去除率 | 13% | 37%(O掺杂) | 95% | [ |
10 | 六氯环三磷腈+硫脲 | P、S | — | 四环素去除率 | 32.95% | 43.48%(P掺杂) 73.50%(S掺杂) | 85.85% | [ |
11 | 三聚氰胺+硫脲+ 磷酸氢二铵 | P、S和O | P取代C1位点 O取代N2位点 S占据间隙位点 | 产氢率 | 467.33μmol·g-1·h-1 | 574μmol·g-1·h-1(S掺杂) 1141μmol·g-1·h-1(P掺杂) | 2479μmol·g-1·h-1 | [ |
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