Chemical Industry and Engineering Progress ›› 2022, Vol. 41 ›› Issue (6): 3293-3305.DOI: 10.16085/j.issn.1000-6613.2021-1493
• Resources and environmental engineering • Previous Articles Next Articles
CHENG Mingqiang(), RU Juanjian(), HUA Yixin, WANG Ding, GENG Xiao, ZHANG Wenwen, HUANG Haoming, WANG Daoxiang
Received:
2021-07-15
Revised:
2021-10-20
Online:
2022-06-21
Published:
2022-06-10
Contact:
RU Juanjian
程明强(), 汝娟坚(), 华一新, 王丁, 耿笑, 张文文, 黄皓铭, 王道祥
通讯作者:
汝娟坚
作者简介:
程明强(1996—),男,硕士研究生,研究方向为锂离子电池材料回收。E-mail:基金资助:
CLC Number:
CHENG Mingqiang, RU Juanjian, HUA Yixin, WANG Ding, GENG Xiao, ZHANG Wenwen, HUANG Haoming, WANG Daoxiang. Progress of deep eutectic solvents in recovery of cathode materials from spent lithium ion batteries[J]. Chemical Industry and Engineering Progress, 2022, 41(6): 3293-3305.
程明强, 汝娟坚, 华一新, 王丁, 耿笑, 张文文, 黄皓铭, 王道祥. 低共熔溶剂在废旧锂离子电池正极材料回收中的研究进展[J]. 化工进展, 2022, 41(6): 3293-3305.
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DESs | HBA/HBD摩尔比 | 密度/g?cm-3 | 黏度/mPa?s | 电导率/mS?cm-1 | 测量温度/℃ | 参考文献 |
---|---|---|---|---|---|---|
氯化胆碱/乙二醇 | 1∶2 | 1.1139 | 25 | 9.73 | 30 | [ |
氯化胆碱/乙二醇 | 1∶2 | 1.12 | 36 | 7.61 | 20 | [ |
氯化胆碱/乙二醇 | 1∶3 | 1.12 | 19 | — | 20 | [ |
氯化胆碱/尿素 | 1∶2 | 1.1879 | 214 | 1.287 | 30 | [ |
氯化胆碱/尿素 | 1∶2 | 1.24 | 169 | 0.199 | 40 | [ |
氯化胆碱/草酸 | 1∶1 | 1.2371 | 89 | 2.35 | 30 | [ |
氯化胆碱/苹果酸 | 1∶1 | 1.2796 | 11475 | 0.041 | 30 | [ |
氯化胆碱/柠檬酸 | 1∶1 | 1.3313 | 45008 | 0.018 | 30 | [ |
氯化胆碱/丙三酸 | 1∶1 | — | 721 | 0.55 | 25 | [ |
氯化胆碱/对甲苯磺酸 | 1∶1 | 1.2074 | 183 | 1.138 | 30 | [ |
氯化胆碱/甘油 | 1∶2 | 1.1854 | 177 | 1.647 | 49 | [ |
氯化胆碱/甘油 | 1∶2 | 1.181 | 376 | 1.047 | — | [ |
氯化胆碱/乙酰胺 | 1∶2 | 1.8052 | 127 | 2.71 | 30 | [ |
DESs | HBA/HBD摩尔比 | 密度/g?cm-3 | 黏度/mPa?s | 电导率/mS?cm-1 | 测量温度/℃ | 参考文献 |
---|---|---|---|---|---|---|
氯化胆碱/乙二醇 | 1∶2 | 1.1139 | 25 | 9.73 | 30 | [ |
氯化胆碱/乙二醇 | 1∶2 | 1.12 | 36 | 7.61 | 20 | [ |
氯化胆碱/乙二醇 | 1∶3 | 1.12 | 19 | — | 20 | [ |
氯化胆碱/尿素 | 1∶2 | 1.1879 | 214 | 1.287 | 30 | [ |
氯化胆碱/尿素 | 1∶2 | 1.24 | 169 | 0.199 | 40 | [ |
氯化胆碱/草酸 | 1∶1 | 1.2371 | 89 | 2.35 | 30 | [ |
氯化胆碱/苹果酸 | 1∶1 | 1.2796 | 11475 | 0.041 | 30 | [ |
氯化胆碱/柠檬酸 | 1∶1 | 1.3313 | 45008 | 0.018 | 30 | [ |
氯化胆碱/丙三酸 | 1∶1 | — | 721 | 0.55 | 25 | [ |
氯化胆碱/对甲苯磺酸 | 1∶1 | 1.2074 | 183 | 1.138 | 30 | [ |
氯化胆碱/甘油 | 1∶2 | 1.1854 | 177 | 1.647 | 49 | [ |
氯化胆碱/甘油 | 1∶2 | 1.181 | 376 | 1.047 | — | [ |
氯化胆碱/乙酰胺 | 1∶2 | 1.8052 | 127 | 2.71 | 30 | [ |
正极活性物质 | DES | 温度/℃ | 时间/h | 固液比/mg·g-1 | 浸出效率/% | 参考文献 | |||
---|---|---|---|---|---|---|---|---|---|
Li | Co | Ni | Mn | ||||||
LiCoO2 | ChCl-EG(1∶2) | 180 | 24 | 20 | 89.8 | 50.3 | — | — | [ |
ChCl-EG(1∶2) | 220 | 24 | 20 | — | 94.1 | — | — | ||
PTSA?1H2O?ChCl | 90 | 15 | 100 | 85 | 88 | — | — | [ | |
PTSA?2H2O?ChCl | 90 | 15 | 100 | 100 | 100 | — | — | ||
PTSA?3H2O?ChCl | 90 | 15 | 100 | 91 | 97 | — | — | ||
ChCl-Urea(1∶2) | 180 | 12 | 20 | 94.7 | 97.9 | — | — | [ | |
ChCl-甲酸(1∶2) | 90 | 12 | 20 | 99.8 | 99.1 | — | — | [ | |
ChCl-乙酸(1∶2) | 90 | 12 | 20 | 63 | 18 | — | — | ||
ChCl-丙酸(1∶2) | 90 | 12 | 20 | 39 | 15 | — | — | ||
ChCl-正丁酸(1∶2) | 90 | 12 | 20 | 33 | 12 | — | — | ||
PEG∶硫脲(1∶2) | 160 | 24 | 20 | — | 71.5 | — | — | [ | |
LiCoO2/Al/Cu Al∶LiCoO2=12%(质量分数) Cu∶LiCoO2=24%(质量分数) | ChCl-CA(1∶1) | 60 | 4 | 20 | — | 99.6 | — | — | [ |
ChCl-EG(1∶1) | 60 | 4 | 20 | — | 2.1 | — | — | ||
ChCl-丙酸(1∶1) | 60 | 4 | 20 | — | 81.2 | — | — | ||
ChCl-丙酸脂(1∶1) | 60 | 4 | 20 | — | 24.4 | — | — | ||
ChCl-OA(1∶1) | 60 | 4 | 20 | — | 19.6 | — | — | ||
ChCl-CA(1∶2) | 40 | 1 | 20 | 93 | 98 | — | — | ||
LiMn2O4 | ChCl-OA(1∶1) | 100 | 0.25 | 16.7 | 99 | 95 | [ | ||
Li a Ni b Mn c Co d O2(a+b+c+d=2) | ChCl-EG(1∶2) | 180 | 24 | 4 | 71 | 32 | 7 | 60 | [ |
LiNi1/3Mn1/3Co1/3O2 | ChCl-EG(1∶2) | 160 | 24 | 20 | — | 90 | — | 10 | [ |
正极活性物质 | DES | 温度/℃ | 时间/h | 固液比/mg·g-1 | 浸出效率/% | 参考文献 | |||
---|---|---|---|---|---|---|---|---|---|
Li | Co | Ni | Mn | ||||||
LiCoO2 | ChCl-EG(1∶2) | 180 | 24 | 20 | 89.8 | 50.3 | — | — | [ |
ChCl-EG(1∶2) | 220 | 24 | 20 | — | 94.1 | — | — | ||
PTSA?1H2O?ChCl | 90 | 15 | 100 | 85 | 88 | — | — | [ | |
PTSA?2H2O?ChCl | 90 | 15 | 100 | 100 | 100 | — | — | ||
PTSA?3H2O?ChCl | 90 | 15 | 100 | 91 | 97 | — | — | ||
ChCl-Urea(1∶2) | 180 | 12 | 20 | 94.7 | 97.9 | — | — | [ | |
ChCl-甲酸(1∶2) | 90 | 12 | 20 | 99.8 | 99.1 | — | — | [ | |
ChCl-乙酸(1∶2) | 90 | 12 | 20 | 63 | 18 | — | — | ||
ChCl-丙酸(1∶2) | 90 | 12 | 20 | 39 | 15 | — | — | ||
ChCl-正丁酸(1∶2) | 90 | 12 | 20 | 33 | 12 | — | — | ||
PEG∶硫脲(1∶2) | 160 | 24 | 20 | — | 71.5 | — | — | [ | |
LiCoO2/Al/Cu Al∶LiCoO2=12%(质量分数) Cu∶LiCoO2=24%(质量分数) | ChCl-CA(1∶1) | 60 | 4 | 20 | — | 99.6 | — | — | [ |
ChCl-EG(1∶1) | 60 | 4 | 20 | — | 2.1 | — | — | ||
ChCl-丙酸(1∶1) | 60 | 4 | 20 | — | 81.2 | — | — | ||
ChCl-丙酸脂(1∶1) | 60 | 4 | 20 | — | 24.4 | — | — | ||
ChCl-OA(1∶1) | 60 | 4 | 20 | — | 19.6 | — | — | ||
ChCl-CA(1∶2) | 40 | 1 | 20 | 93 | 98 | — | — | ||
LiMn2O4 | ChCl-OA(1∶1) | 100 | 0.25 | 16.7 | 99 | 95 | [ | ||
Li a Ni b Mn c Co d O2(a+b+c+d=2) | ChCl-EG(1∶2) | 180 | 24 | 4 | 71 | 32 | 7 | 60 | [ |
LiNi1/3Mn1/3Co1/3O2 | ChCl-EG(1∶2) | 160 | 24 | 20 | — | 90 | — | 10 | [ |
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