Chemical Industry and Engineering Progress ›› 2023, Vol. 42 ›› Issue (7): 3834-3846.DOI: 10.16085/j.issn.1000-6613.2022-1582
• Resources and environmental engineering • Previous Articles Next Articles
BAI Yadi1,2(), DENG Shuai1,2(), ZHAO Ruikai1,2, ZHAO Li1, YANG Yingxia3
Received:
2022-08-26
Revised:
2022-11-15
Online:
2023-08-14
Published:
2023-07-15
Contact:
DENG Shuai
白亚迪1,2(), 邓帅1,2(), 赵睿恺1,2, 赵力1, 杨英霞3
通讯作者:
邓帅
作者简介:
白亚迪(1998—),男,硕士研究生,研究方向为二氧化碳吸附。E-mail:1571071872@qq.com。
基金资助:
CLC Number:
BAI Yadi, DENG Shuai, ZHAO Ruikai, ZHAO Li, YANG Yingxia. Exploration on standardized test scheme and experimental performance of temperature swing adsorption carbon capture unit[J]. Chemical Industry and Engineering Progress, 2023, 42(7): 3834-3846.
白亚迪, 邓帅, 赵睿恺, 赵力, 杨英霞. 变温吸附碳捕集机组标准化测试方案探讨及性能实验[J]. 化工进展, 2023, 42(7): 3834-3846.
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URL: https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2022-1582
参考文献 | 技术类型 | 研究方法 | 单位能耗/MJ·kg-1 | e1 | e2 | e3 | e4 | e5 | e6 | e7 | e8 |
---|---|---|---|---|---|---|---|---|---|---|---|
Liu等[ | TSA | 实验 | 8.41 | √ | √ | √ | √ | √ | |||
Ntiamoah等[ | TSA | 实验 | 3.4 | √ | √ | ||||||
Chen等[ | TSA | 模拟 | 5.36 | √ | √ | √ | √ | ||||
Marx等[ | TSA | 模拟 | 2.85 | √ | √ | √ | |||||
TSA | 模拟 | 12.6 | √ | √ | √ | √ | |||||
Jiang等[ | TSA | 模拟 | 6.76 | √ | √ | √ | |||||
TVSA | 模拟 | 3.22 | √ | √ | √ | √ | |||||
Ben-Mansour等[ | TSA | 模拟 | 2.39 | √ | √ | √ | √ |
参考文献 | 技术类型 | 研究方法 | 单位能耗/MJ·kg-1 | e1 | e2 | e3 | e4 | e5 | e6 | e7 | e8 |
---|---|---|---|---|---|---|---|---|---|---|---|
Liu等[ | TSA | 实验 | 8.41 | √ | √ | √ | √ | √ | |||
Ntiamoah等[ | TSA | 实验 | 3.4 | √ | √ | ||||||
Chen等[ | TSA | 模拟 | 5.36 | √ | √ | √ | √ | ||||
Marx等[ | TSA | 模拟 | 2.85 | √ | √ | √ | |||||
TSA | 模拟 | 12.6 | √ | √ | √ | √ | |||||
Jiang等[ | TSA | 模拟 | 6.76 | √ | √ | √ | |||||
TVSA | 模拟 | 3.22 | √ | √ | √ | √ | |||||
Ben-Mansour等[ | TSA | 模拟 | 2.39 | √ | √ | √ | √ |
进气体积分数 | 进气温度 | 热源温度 | 冷源温度 | 环境温度 | 气体流速 |
---|---|---|---|---|---|
15% CO2 85% N2 | 25℃ | 160℃ | 25℃ | 25℃ | 根据吸附剂的材质、结构和性能确定:采用颗粒状活性炭时,为0.20~0.60m/s;采用活性炭纤维毡时,为0.10~0.15m/s;采用蜂窝状吸附剂时,为0.70~1.20m/s |
进气体积分数 | 进气温度 | 热源温度 | 冷源温度 | 环境温度 | 气体流速 |
---|---|---|---|---|---|
15% CO2 85% N2 | 25℃ | 160℃ | 25℃ | 25℃ | 根据吸附剂的材质、结构和性能确定:采用颗粒状活性炭时,为0.20~0.60m/s;采用活性炭纤维毡时,为0.10~0.15m/s;采用蜂窝状吸附剂时,为0.70~1.20m/s |
能耗项 | 计算公式 | 含义 | 备注 |
---|---|---|---|
E1 | 加热过程中吸附剂升温所消耗的能量 | ms为吸附剂质量;cp,s为吸附剂的比热容;Tads和Tdes分别为吸附和解吸温度 | |
E2 | CO2和N2从吸附剂中脱附时消耗的能量 | ||
E3 | 解吸出的CO2和N2被加热所消耗的能量 | ||
E4+E5 | 吸附腔金属壁面升温及其向环境的散热所消耗的能量 | t1为加热时间;qoil为导热介质流量;cp,oil为导热介质比热;ΔT1为吸附腔两端的温差 | |
E6+E7 | 导热介质输送管道升温及其向环境散热所消耗的能量 | ΔT2为热源两端的温差 | |
E8 | 真空泵等运行所消耗的能量 | t2为泵工作时间;P为泵功率 |
能耗项 | 计算公式 | 含义 | 备注 |
---|---|---|---|
E1 | 加热过程中吸附剂升温所消耗的能量 | ms为吸附剂质量;cp,s为吸附剂的比热容;Tads和Tdes分别为吸附和解吸温度 | |
E2 | CO2和N2从吸附剂中脱附时消耗的能量 | ||
E3 | 解吸出的CO2和N2被加热所消耗的能量 | ||
E4+E5 | 吸附腔金属壁面升温及其向环境的散热所消耗的能量 | t1为加热时间;qoil为导热介质流量;cp,oil为导热介质比热;ΔT1为吸附腔两端的温差 | |
E6+E7 | 导热介质输送管道升温及其向环境散热所消耗的能量 | ΔT2为热源两端的温差 | |
E8 | 真空泵等运行所消耗的能量 | t2为泵工作时间;P为泵功率 |
性能指标所需测量参数 | 纯度 | 回收率 | 比能耗 | 能源效率 |
---|---|---|---|---|
解吸阶段出口处实时气体流量 | √ | √ | √ | √ |
吸附阶段进口处的气体流量 | √ | √ | ||
气体中实时CO2含量 | √ | √ | √ | √ |
进出机组及吸附腔的导热介质温度 | √ | √ | ||
环境温度 | √ | √ | ||
吸附剂温度 | √ | √ | ||
导热介质流量 | √ | √ | ||
泵实时功率 | √ | √ | ||
气体吸附热 | Δ | Δ | ||
相应温度下气体的焓 | ○ | ○ | ||
分离前后CO2相应的熵变和焓变 | ○ |
性能指标所需测量参数 | 纯度 | 回收率 | 比能耗 | 能源效率 |
---|---|---|---|---|
解吸阶段出口处实时气体流量 | √ | √ | √ | √ |
吸附阶段进口处的气体流量 | √ | √ | ||
气体中实时CO2含量 | √ | √ | √ | √ |
进出机组及吸附腔的导热介质温度 | √ | √ | ||
环境温度 | √ | √ | ||
吸附剂温度 | √ | √ | ||
导热介质流量 | √ | √ | ||
泵实时功率 | √ | √ | ||
气体吸附热 | Δ | Δ | ||
相应温度下气体的焓 | ○ | ○ | ||
分离前后CO2相应的熵变和焓变 | ○ |
参数 | 数值 | 参数 | 数值 |
---|---|---|---|
吸附腔高度/mm | 1100 | 翅片间距/mm | 5 |
吸附腔外径/mm | 100 | 翅片厚度/mm | 1 |
吸附腔壁厚/mm | 5 | 管路外径/mm | 12 |
换热管外径/mm | 12 | 管路壁厚/mm | 1 |
换热管壁厚/mm | 1 | 每腔吸附剂填充量/kg | 5 |
翅片高度/mm | 7 |
参数 | 数值 | 参数 | 数值 |
---|---|---|---|
吸附腔高度/mm | 1100 | 翅片间距/mm | 5 |
吸附腔外径/mm | 100 | 翅片厚度/mm | 1 |
吸附腔壁厚/mm | 5 | 管路外径/mm | 12 |
换热管外径/mm | 12 | 管路壁厚/mm | 1 |
换热管壁厚/mm | 1 | 每腔吸附剂填充量/kg | 5 |
翅片高度/mm | 7 |
测量位置 | 测试参数 | 测试设备 | 准确度 |
---|---|---|---|
T1~T10 | 温度/℃ | K型热电偶 | ±0.75%RDG |
T11~T18 | Pt100 | ±0.25%RDG | |
P1、P2 | 压力/MPa | 压力传感器 | ±1%RDG |
HC1、HC2 | 冷/热量/MJ | 热量积算仪 | ±0.2%RDG |
PM | 功率/W | 功率表 | ±0.4%RDG +±0.1%F.S. |
MF1、MF2 | 气体流量/L·min-1 | 热式质量流量计 | ±0.5%RDG +±0.3%F.S. |
RM1、RM2、RM3 | 带流量调节功能的流量计 | ||
D1、D2、D3 | CO2体积分数/% | CO2检测仪 | ≤±1%F.S. |
测量位置 | 测试参数 | 测试设备 | 准确度 |
---|---|---|---|
T1~T10 | 温度/℃ | K型热电偶 | ±0.75%RDG |
T11~T18 | Pt100 | ±0.25%RDG | |
P1、P2 | 压力/MPa | 压力传感器 | ±1%RDG |
HC1、HC2 | 冷/热量/MJ | 热量积算仪 | ±0.2%RDG |
PM | 功率/W | 功率表 | ±0.4%RDG +±0.1%F.S. |
MF1、MF2 | 气体流量/L·min-1 | 热式质量流量计 | ±0.5%RDG +±0.3%F.S. |
RM1、RM2、RM3 | 带流量调节功能的流量计 | ||
D1、D2、D3 | CO2体积分数/% | CO2检测仪 | ≤±1%F.S. |
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