Chemical Industry and Engineering Progress ›› 2023, Vol. 42 ›› Issue (5): 2666-2677.DOI: 10.16085/j.issn.1000-6613.2022-1314
• Resources and environmental engineering • Previous Articles Next Articles
LI Weihua1(), WU Yinkai1, SUN Yingjie1(), YIN Junquan1, XIN Mingxue1, ZHAO Youjie2
Received:
2022-07-12
Revised:
2022-08-16
Online:
2023-06-02
Published:
2023-05-10
Contact:
SUN Yingjie
李卫华1(), 吴寅凯1, 孙英杰1(), 尹俊权1, 辛明学1, 赵友杰2
通讯作者:
孙英杰
作者简介:
李卫华(1989—),男,副教授,研究方向为垃圾焚烧飞灰污染控制与资源化。E-mail:liweihua@qut.edu.cn。
基金资助:
CLC Number:
LI Weihua, WU Yinkai, SUN Yingjie, YIN Junquan, XIN Mingxue, ZHAO Youjie. Progress on evaluation methods for toxic leaching of heavy metals from MSW incineration fly ash[J]. Chemical Industry and Engineering Progress, 2023, 42(5): 2666-2677.
李卫华, 吴寅凯, 孙英杰, 尹俊权, 辛明学, 赵友杰. 垃圾焚烧飞灰重金属毒性浸出评价方法研究进展[J]. 化工进展, 2023, 42(5): 2666-2677.
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方法名称 | 编号 | 国家 | 现行情况 |
---|---|---|---|
提取程序:毒性试验方法和结构完整性试验 | US EPA 1310B (EP) | 美国 | 现行 |
毒性特征浸出程序 | US EPA 1311 (TCLP) | 美国 | 现行 |
合成沉淀浸出程序 | US EPA 1312 (SPLP) | 美国 | 现行 |
多级提取程序 | US EPA 1320 (MEP) | 美国 | 现行 |
废弃物单批次提取法的标准试验方法 | US ASTM D 5233 | 美国 | 现行 |
水振荡提取固体废物的标准实施规程 | US ASTM D 3987 | 美国 | 现行 |
水连续分批次提取废物的标准试验方法 | US ASTM D 4793 | 美国 | 现行 |
基于柱状设备浸出固体物质的标准试验方法 | US ASTM D 4874 | 美国 | 现行 |
酸性萃取液连续分批次提取废物的标准试验方法 | US ASTM D 5284 | 美国 | 现行 |
废弃物的表征—浸出行为试验—上流式渗透试验 | BS EN 14405 | 欧盟 | 现行 |
废弃物的特性—浸出—颗粒废弃物和污泥的一致性试验 | BS EN 12457 | 欧盟 | 现行 |
浸出特性—无机成分浸出有效性测定—固体泥土和石质材料 | NEN 7371 | 荷兰 | 现行 |
浸出特性—基于扩散试验的模制或整体材料中无机成分的浸出测定—固体土和石质材料 | NEN 7375 | 荷兰 | 现行 |
日本环境省第13号告示 | JLT 13 | 日本 | 现行 |
固体废物 浸出毒性浸出方法 醋酸缓冲溶液法 | HJ/T 300-2007 | 中国 | 现行 |
固体废物 浸出毒性浸出方法 硫酸硝酸法 | HJ/T 299-2007 | 中国 | 现行 |
固体废物 浸出毒性浸出方法 水平振荡法 | HJ 557-2010 | 中国 | 现行 |
方法名称 | 编号 | 国家 | 现行情况 |
---|---|---|---|
提取程序:毒性试验方法和结构完整性试验 | US EPA 1310B (EP) | 美国 | 现行 |
毒性特征浸出程序 | US EPA 1311 (TCLP) | 美国 | 现行 |
合成沉淀浸出程序 | US EPA 1312 (SPLP) | 美国 | 现行 |
多级提取程序 | US EPA 1320 (MEP) | 美国 | 现行 |
废弃物单批次提取法的标准试验方法 | US ASTM D 5233 | 美国 | 现行 |
水振荡提取固体废物的标准实施规程 | US ASTM D 3987 | 美国 | 现行 |
水连续分批次提取废物的标准试验方法 | US ASTM D 4793 | 美国 | 现行 |
基于柱状设备浸出固体物质的标准试验方法 | US ASTM D 4874 | 美国 | 现行 |
酸性萃取液连续分批次提取废物的标准试验方法 | US ASTM D 5284 | 美国 | 现行 |
废弃物的表征—浸出行为试验—上流式渗透试验 | BS EN 14405 | 欧盟 | 现行 |
废弃物的特性—浸出—颗粒废弃物和污泥的一致性试验 | BS EN 12457 | 欧盟 | 现行 |
浸出特性—无机成分浸出有效性测定—固体泥土和石质材料 | NEN 7371 | 荷兰 | 现行 |
浸出特性—基于扩散试验的模制或整体材料中无机成分的浸出测定—固体土和石质材料 | NEN 7375 | 荷兰 | 现行 |
日本环境省第13号告示 | JLT 13 | 日本 | 现行 |
固体废物 浸出毒性浸出方法 醋酸缓冲溶液法 | HJ/T 300-2007 | 中国 | 现行 |
固体废物 浸出毒性浸出方法 硫酸硝酸法 | HJ/T 299-2007 | 中国 | 现行 |
固体废物 浸出毒性浸出方法 水平振荡法 | HJ 557-2010 | 中国 | 现行 |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
US EPA 1310B (EP) | 0.5mol/L的乙酸溶液 | (16~20)∶1 | 无要求 | 1 | 24 |
TCLP | pH=2.88±0.05的乙酸溶液 | 20∶1(质量比) | <9.5 | 1 | 18±2 |
ASTM D 5233 | pH=2.88±0.05的乙酸溶液 | 20∶1(质量比) | 无要求 | 1 | 18±2 |
HJ/T 300—2007 | pH=2.64±0.05的乙酸溶液 | 20∶1(L/kg) | <9.5 | 1 | 18±2 |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
US EPA 1310B (EP) | 0.5mol/L的乙酸溶液 | (16~20)∶1 | 无要求 | 1 | 24 |
TCLP | pH=2.88±0.05的乙酸溶液 | 20∶1(质量比) | <9.5 | 1 | 18±2 |
ASTM D 5233 | pH=2.88±0.05的乙酸溶液 | 20∶1(质量比) | 无要求 | 1 | 18±2 |
HJ/T 300—2007 | pH=2.64±0.05的乙酸溶液 | 20∶1(L/kg) | <9.5 | 1 | 18±2 |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
SPLP | 试剂水加质量比为60/40的硫酸和硝酸混合液 | 20∶1(质量比) | <9.5 | 1 | 18±2 |
MEP | 试剂水加质量比为60/40的硫酸和硝酸混合液,pH为3.0±0.2 | 20∶1(质量比) | <9.5 | 10+ | 24 (单次) |
HJ/T 299—2007 | 试剂水加质量比为2∶1的硫酸和硝酸,pH为3.20±0.05 | 10∶1(L/kg) | <9.5 | 1 | 18±2 |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
SPLP | 试剂水加质量比为60/40的硫酸和硝酸混合液 | 20∶1(质量比) | <9.5 | 1 | 18±2 |
MEP | 试剂水加质量比为60/40的硫酸和硝酸混合液,pH为3.0±0.2 | 20∶1(质量比) | <9.5 | 10+ | 24 (单次) |
HJ/T 299—2007 | 试剂水加质量比为2∶1的硫酸和硝酸,pH为3.20±0.05 | 10∶1(L/kg) | <9.5 | 1 | 18±2 |
方法 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|
BS EN 12457-1 | 2∶1(L/kg) | <4 | 1 | 24±0.5 |
BS EN 12457-2 | 10∶1(L/kg) | <4 | 1 | 24±0.5 |
BS EN 12457-3 | 2∶1(L/kg) 8∶1(L/kg) | <4 | 2 | 6±0.5 18±0.5 |
BS EN 12457-4 | 10∶1(L/kg) | <10 | 1 | 24±0.5 |
方法 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|
BS EN 12457-1 | 2∶1(L/kg) | <4 | 1 | 24±0.5 |
BS EN 12457-2 | 10∶1(L/kg) | <4 | 1 | 24±0.5 |
BS EN 12457-3 | 2∶1(L/kg) 8∶1(L/kg) | <4 | 2 | 6±0.5 18±0.5 |
BS EN 12457-4 | 10∶1(L/kg) | <10 | 1 | 24±0.5 |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
ASTM D 3987 | 试剂水 | 20∶1(v/w) | 无要求 | 1 | 18±0.25 |
ASTM D 4793 | 试剂水 | 20∶1(v/w) | 无要求 | 10 | 18±0.25(单次) |
ASTM D 4874 | 试剂水 | — | ≤10 | — | — |
ASTM D 5284 | 质量比为60/40的硫酸和硝酸混合液 | 20∶1(v/w) | 无要求 | 10 | 18±0.25(单次) |
方法 | 浸提剂 | 液固比 | 样品粒径/mm | 浸提次数 | 浸出时间/h |
---|---|---|---|---|---|
ASTM D 3987 | 试剂水 | 20∶1(v/w) | 无要求 | 1 | 18±0.25 |
ASTM D 4793 | 试剂水 | 20∶1(v/w) | 无要求 | 10 | 18±0.25(单次) |
ASTM D 4874 | 试剂水 | — | ≤10 | — | — |
ASTM D 5284 | 质量比为60/40的硫酸和硝酸混合液 | 20∶1(v/w) | 无要求 | 10 | 18±0.25(单次) |
方法 | 浸提剂 | 液固比 | 样品粒径 | 浸提次数 | 浸出时间 |
---|---|---|---|---|---|
NEN 7371 | 中性水和硝酸,两次浸提将pH调节为7和4 | 50∶1(质量比) | <125μm | 2 | 3h(单次) |
NEN 7375 | 脱矿中性水 | 20∶1(体积质量比) | ≥40mm | 8 | 64d(总共) |
方法 | 浸提剂 | 液固比 | 样品粒径 | 浸提次数 | 浸出时间 |
---|---|---|---|---|---|
NEN 7371 | 中性水和硝酸,两次浸提将pH调节为7和4 | 50∶1(质量比) | <125μm | 2 | 3h(单次) |
NEN 7375 | 脱矿中性水 | 20∶1(体积质量比) | ≥40mm | 8 | 64d(总共) |
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