Chemical Industry and Engineering Progress ›› 2025, Vol. 44 ›› Issue (3): 1607-1618.DOI: 10.16085/j.issn.1000-6613.2024-0398
• Materials science and technology • Previous Articles Next Articles
BAI Zhongliang1(
), LI Ping1(
), WANG Hui1, LI Wei1, ZHANG Qiang2, LI Ning3
Received:2024-03-11
Revised:2024-04-15
Online:2025-04-15
Published:2025-03-25
Contact:
LI Ping
白中良1(
), 李萍1(
), 王晖1, 李伟1, 张强2, 李宁3
通讯作者:
李萍
作者简介:白中良(1998—),男,硕士研究生,研究方向为沥青再生剂研发。E-mail:13609325481@163.com。
基金资助:CLC Number:
BAI Zhongliang, LI Ping, WANG Hui, LI Wei, ZHANG Qiang, LI Ning. Proportioning design and anti-aging performance of asphalt rejuvenator based on response surface methodology[J]. Chemical Industry and Engineering Progress, 2025, 44(3): 1607-1618.
白中良, 李萍, 王晖, 李伟, 张强, 李宁. 基于响应曲面法的沥青再生剂配比设计以及抗老化性能[J]. 化工进展, 2025, 44(3): 1607-1618.
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URL: https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2024-0398
| 技术指标 | 糠醛抽出油 | 废机油 |
|---|---|---|
| 黏度(60℃)/mm2·s-1 | 2105 | 25.42 |
| 闪点/℃ | 266 | 226 |
| 质量损失/% | -0.408 | -5.509 |
| 密度(15℃)/g·cm-3 | 0.86 | 0.83 |
| 饱和分/% | 18 | 49 |
| 芳香分/% | 36 | 27 |
| 技术指标 | 糠醛抽出油 | 废机油 |
|---|---|---|
| 黏度(60℃)/mm2·s-1 | 2105 | 25.42 |
| 闪点/℃ | 266 | 226 |
| 质量损失/% | -0.408 | -5.509 |
| 密度(15℃)/g·cm-3 | 0.86 | 0.83 |
| 饱和分/% | 18 | 49 |
| 芳香分/% | 36 | 27 |
| 技术指标 | ATBC | DOP | DBP |
|---|---|---|---|
| 闪点/℃ | 201.0 | 205.1 | 185.0 |
| 酯质量分数/% | 99.4 | 99.5 | 99.5 |
| 水分质量分数/% | 0.04 | 0.05 | 0.10 |
| 密度(15℃)/g·cm-3 | 1.052 | 0.986 | 1.002 |
| 酸值(以KOH计)/mg·g-1 | 0.040 | 0.003 | 0.100 |
| 色度 | 15 | 30 | 25 |
| 技术指标 | ATBC | DOP | DBP |
|---|---|---|---|
| 闪点/℃ | 201.0 | 205.1 | 185.0 |
| 酯质量分数/% | 99.4 | 99.5 | 99.5 |
| 水分质量分数/% | 0.04 | 0.05 | 0.10 |
| 密度(15℃)/g·cm-3 | 1.052 | 0.986 | 1.002 |
| 酸值(以KOH计)/mg·g-1 | 0.040 | 0.003 | 0.100 |
| 色度 | 15 | 30 | 25 |
| 技术指标 | C5石油树脂 | C9石油树脂 |
|---|---|---|
| 外观 | 浅黄颗粒 | 浅黄颗粒 |
| 色号 | 4 | 4 |
| 软化点/℃ | 102.5 | 112.0 |
| 酸值/mg KOH·g-1 | 0.9 | 0.9 |
| 灰分/% | 0.07 | 0.08 |
| 溴值/g Br·100g-1 | 15 | 17 |
| 技术指标 | C5石油树脂 | C9石油树脂 |
|---|---|---|
| 外观 | 浅黄颗粒 | 浅黄颗粒 |
| 色号 | 4 | 4 |
| 软化点/℃ | 102.5 | 112.0 |
| 酸值/mg KOH·g-1 | 0.9 | 0.9 |
| 灰分/% | 0.07 | 0.08 |
| 溴值/g Br·100g-1 | 15 | 17 |
| 技术指标 | ZH-90# | ZH-90#(RTFOT85min) | ZH-90#(氙灯老化22.4d) | ZH-90#(PAV20h) |
|---|---|---|---|---|
| 针入度(25℃)/0.01mm | 84.0 | 55.2 | 43.9 | 25.9 |
| 软化点/℃ | 45.8 | 50.8 | 49.6 | 60.7 |
| 延度(10℃)/cm | 135.8 | 9.4 | 4.4 | 2.2 |
| 黏度(135℃)/Pa·s | 0.422 | 0.594 | 0.692 | 1.046 |
| 技术指标 | ZH-90# | ZH-90#(RTFOT85min) | ZH-90#(氙灯老化22.4d) | ZH-90#(PAV20h) |
|---|---|---|---|---|
| 针入度(25℃)/0.01mm | 84.0 | 55.2 | 43.9 | 25.9 |
| 软化点/℃ | 45.8 | 50.8 | 49.6 | 60.7 |
| 延度(10℃)/cm | 135.8 | 9.4 | 4.4 | 2.2 |
| 黏度(135℃)/Pa·s | 0.422 | 0.594 | 0.692 | 1.046 |
| 沥青类型 | 针入度下降率/% | 黏度增加率/% |
|---|---|---|
| ZH-90# (RTFOT85min) | 34.29 | 40.76 |
| ZH-90# (氙灯老化22.4d) | 47.74 | 63.98 |
| ZH-90# (PAV20h) | 69.17 | 147.87 |
| 沥青类型 | 针入度下降率/% | 黏度增加率/% |
|---|---|---|
| ZH-90# (RTFOT85min) | 34.29 | 40.76 |
| ZH-90# (氙灯老化22.4d) | 47.74 | 63.98 |
| ZH-90# (PAV20h) | 69.17 | 147.87 |
| 序号 | 基础油分 | 增塑剂 | 增黏树脂 |
|---|---|---|---|
| 1 | 废机油(A1) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 2 | 废机油(A1) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 3 | 废机油(A1) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 4 | 废机油(A1) | 邻苯二甲酸二辛酯(B1) | C9石油树脂(C2) |
| 5 | 废机油(A1) | 乙酰基柠檬酸三丁酯(B2) | C9石油树脂(C2) |
| 6 | 废机油(A1) | 邻苯二甲酸二丁酯(B3) | C9石油树脂(C2) |
| 7 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 8 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 9 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 10 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C9石油树脂(C2) |
| 11 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C9石油树脂(C2) |
| 12 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C9石油树脂(C2) |
| 序号 | 基础油分 | 增塑剂 | 增黏树脂 |
|---|---|---|---|
| 1 | 废机油(A1) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 2 | 废机油(A1) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 3 | 废机油(A1) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 4 | 废机油(A1) | 邻苯二甲酸二辛酯(B1) | C9石油树脂(C2) |
| 5 | 废机油(A1) | 乙酰基柠檬酸三丁酯(B2) | C9石油树脂(C2) |
| 6 | 废机油(A1) | 邻苯二甲酸二丁酯(B3) | C9石油树脂(C2) |
| 7 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 8 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 9 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 10 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C9石油树脂(C2) |
| 11 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C9石油树脂(C2) |
| 12 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C9石油树脂(C2) |
| 沥青老化程度 | 基础油分 | 增塑剂 | 增黏树脂 |
|---|---|---|---|
| 轻度 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 中度 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 重度 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 沥青老化程度 | 基础油分 | 增塑剂 | 增黏树脂 |
|---|---|---|---|
| 轻度 | 糠醛抽出油(A2) | 邻苯二甲酸二丁酯(B3) | C5石油树脂(C1) |
| 中度 | 糠醛抽出油(A2) | 乙酰基柠檬酸三丁酯(B2) | C5石油树脂(C1) |
| 重度 | 糠醛抽出油(A2) | 邻苯二甲酸二辛酯(B1) | C5石油树脂(C1) |
| 编号 | 实验点类型 | X1 | X2 |
|---|---|---|---|
| 1 | 各个影响因子的 实验设计点mc | 1 | 1 |
| 2 | 1 | -1 | |
| 3 | -1 | 1 | |
| 4 | -1 | -1 | |
| 5 | 中心点m0 | 0 | 0 |
| 6 | 0 | 0 | |
| 7 | 0 | 0 | |
| 8 | 0 | 0 | |
| 9 | 0 | 0 | |
| 10 | 轴向点mr | r | 0 |
| 11 | 0 | r | |
| 12 | -r | 0 | |
| 13 | 0 | -r |
| 编号 | 实验点类型 | X1 | X2 |
|---|---|---|---|
| 1 | 各个影响因子的 实验设计点mc | 1 | 1 |
| 2 | 1 | -1 | |
| 3 | -1 | 1 | |
| 4 | -1 | -1 | |
| 5 | 中心点m0 | 0 | 0 |
| 6 | 0 | 0 | |
| 7 | 0 | 0 | |
| 8 | 0 | 0 | |
| 9 | 0 | 0 | |
| 10 | 轴向点mr | r | 0 |
| 11 | 0 | r | |
| 12 | -r | 0 | |
| 13 | 0 | -r |
| 种类 | 编号 | X1/% | X2/% | Y1/0.1mm | Y2/Pa·s | Y3/cm | Y4/℃ |
|---|---|---|---|---|---|---|---|
| 轻度老化 | 1 | 5.00 | 5.85 | 71.8 | 199.8 | 43.7 | 44.8 |
| 2 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 3 | 8.00 | 10.00 | 80.0 | 190.5 | 67.5 | 44.8 | |
| 4 | 2.00 | 10.00 | 80.4 | 187.5 | 84.2 | 44.3 | |
| 5 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 6 | 0.76 | 20.00 | 87.7 | 182.9 | 134.1 | 43.1 | |
| 7 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 8 | 9.24 | 20.00 | 79.4 | 188.8 | 85.2 | 44.1 | |
| 9 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 10 | 8.00 | 30.00 | 90.4 | 180.3 | 119.0 | 43.2 | |
| 11 | 2.00 | 30.00 | 91.3 | 177.8 | 120.1 | 41.2 | |
| 12 | 5.00 | 34.14 | 85.3 | 178.7 | 115.7 | 44.1 | |
| 13 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 中度老化 | 1 | 1.50 | 10.00 | 85.6 | 190.1 | 106.7 | 43.5 |
| 2 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 3 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 4 | 4.00 | 46.21 | 90.1 | 167.2 | 109.4 | 42.4 | |
| 5 | 6.50 | 10.00 | 76.7 | 221.1 | 35.9 | 45.2 | |
| 6 | 7.54 | 25.00 | 84.0 | 195.1 | 80.6 | 43.0 | |
| 7 | 4.00 | 3.79 | 66.1 | 279.4 | 27.2 | 44.9 | |
| 8 | 6.50 | 40.00 | 92.6 | 141.3 | 114.8 | 42.7 | |
| 9 | 0.46 | 25.00 | 86.1 | 187.5 | 119.2 | 42.4 | |
| 10 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 11 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 12 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 13 | 1.50 | 40.00 | 87.6 | 164.3 | 103.2 | 43.2 | |
| 重度老化 | 1 | 4.34 | 11.59 | 63.9 | 423.3 | 27.9 | 46.3 |
| 2 | 5.00 | 27.50 | 75.4 | 355.0 | 29.7 | 45.6 | |
| 3 | 4.34 | 43.41 | 81.7 | 285.0 | 41.2 | 44.1 | |
| 4 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 5 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 6 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 7 | 2.75 | 50.00 | 86.0 | 281.9 | 45.0 | 43.3 | |
| 8 | 1.16 | 43.41 | 87.9 | 306.9 | 44.6 | 43.8 | |
| 9 | 2.75 | 5.00 | 63.9 | 441.7 | 26.8 | 46.6 | |
| 10 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 11 | 0.50 | 27.50 | 78.3 | 330.0 | 31.6 | 44.4 | |
| 12 | 1.16 | 11.59 | 69.3 | 360.0 | 29.4 | 44.9 | |
| 13 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 |
| 种类 | 编号 | X1/% | X2/% | Y1/0.1mm | Y2/Pa·s | Y3/cm | Y4/℃ |
|---|---|---|---|---|---|---|---|
| 轻度老化 | 1 | 5.00 | 5.85 | 71.8 | 199.8 | 43.7 | 44.8 |
| 2 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 3 | 8.00 | 10.00 | 80.0 | 190.5 | 67.5 | 44.8 | |
| 4 | 2.00 | 10.00 | 80.4 | 187.5 | 84.2 | 44.3 | |
| 5 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 6 | 0.76 | 20.00 | 87.7 | 182.9 | 134.1 | 43.1 | |
| 7 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 8 | 9.24 | 20.00 | 79.4 | 188.8 | 85.2 | 44.1 | |
| 9 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 10 | 8.00 | 30.00 | 90.4 | 180.3 | 119.0 | 43.2 | |
| 11 | 2.00 | 30.00 | 91.3 | 177.8 | 120.1 | 41.2 | |
| 12 | 5.00 | 34.14 | 85.3 | 178.7 | 115.7 | 44.1 | |
| 13 | 5.00 | 20.00 | 84.5 | 186.1 | 94.7 | 44.3 | |
| 中度老化 | 1 | 1.50 | 10.00 | 85.6 | 190.1 | 106.7 | 43.5 |
| 2 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 3 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 4 | 4.00 | 46.21 | 90.1 | 167.2 | 109.4 | 42.4 | |
| 5 | 6.50 | 10.00 | 76.7 | 221.1 | 35.9 | 45.2 | |
| 6 | 7.54 | 25.00 | 84.0 | 195.1 | 80.6 | 43.0 | |
| 7 | 4.00 | 3.79 | 66.1 | 279.4 | 27.2 | 44.9 | |
| 8 | 6.50 | 40.00 | 92.6 | 141.3 | 114.8 | 42.7 | |
| 9 | 0.46 | 25.00 | 86.1 | 187.5 | 119.2 | 42.4 | |
| 10 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 11 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 12 | 4.00 | 25.00 | 80.9 | 204.2 | 54.0 | 43.4 | |
| 13 | 1.50 | 40.00 | 87.6 | 164.3 | 103.2 | 43.2 | |
| 重度老化 | 1 | 4.34 | 11.59 | 63.9 | 423.3 | 27.9 | 46.3 |
| 2 | 5.00 | 27.50 | 75.4 | 355.0 | 29.7 | 45.6 | |
| 3 | 4.34 | 43.41 | 81.7 | 285.0 | 41.2 | 44.1 | |
| 4 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 5 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 6 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 7 | 2.75 | 50.00 | 86.0 | 281.9 | 45.0 | 43.3 | |
| 8 | 1.16 | 43.41 | 87.9 | 306.9 | 44.6 | 43.8 | |
| 9 | 2.75 | 5.00 | 63.9 | 441.7 | 26.8 | 46.6 | |
| 10 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 | |
| 11 | 0.50 | 27.50 | 78.3 | 330.0 | 31.6 | 44.4 | |
| 12 | 1.16 | 11.59 | 69.3 | 360.0 | 29.4 | 44.9 | |
| 13 | 2.75 | 27.50 | 76.8 | 335.0 | 31.2 | 44.5 |
| 响应指标 | 期望值 |
|---|---|
| 针入度(25℃)/0.1mm | 80~100 |
| 黏度(60℃)/Pa·s | ≥160 |
| 延度(10℃)/cm | ≥30 |
| 软化点/℃ | ≥44 |
| 响应指标 | 期望值 |
|---|---|
| 针入度(25℃)/0.1mm | 80~100 |
| 黏度(60℃)/Pa·s | ≥160 |
| 延度(10℃)/cm | ≥30 |
| 软化点/℃ | ≥44 |
| 再生剂类型 | 影响因子最优值 | 响应指标最优值 | ||||
|---|---|---|---|---|---|---|
| X1/% | X2/% | Y1/0.1mm | Y2/Pa·s | Y3/cm | Y4/℃ | |
| 轻度老化 | 6.79 | 19.34 | 83.4 | 187.2 | 89.4 | 44.5 |
| 中度老化 | 5.65 | 24.10 | 81.2 | 202.4 | 53.1 | 44.1 |
| 重度老化 | 1.16 | 33.50 | 81.9 | 317.0 | 35.7 | 44.0 |
| 再生剂类型 | 影响因子最优值 | 响应指标最优值 | ||||
|---|---|---|---|---|---|---|
| X1/% | X2/% | Y1/0.1mm | Y2/Pa·s | Y3/cm | Y4/℃ | |
| 轻度老化 | 6.79 | 19.34 | 83.4 | 187.2 | 89.4 | 44.5 |
| 中度老化 | 5.65 | 24.10 | 81.2 | 202.4 | 53.1 | 44.1 |
| 重度老化 | 1.16 | 33.50 | 81.9 | 317.0 | 35.7 | 44.0 |
| 种类 | 编号 | X3/% | X4/% | Y5/% | Y6/% | Y7/cm | Y8/0.1mm |
|---|---|---|---|---|---|---|---|
轻度 老化 | 1 | 0.60 | 0.60 | 66.49 | -0.47 | 12.0 | 82.9 |
| 2 | 2.20 | 0.60 | 62.66 | -0.49 | 9.2 | 81.6 | |
| 3 | 0.60 | 2.20 | 67.70 | -0.52 | 12.4 | 83.2 | |
| 4 | 2.20 | 2.20 | 61.44 | -0.52 | 10.1 | 81.7 | |
| 5 | 0.27 | 1.40 | 63.20 | -0.40 | 10.7 | 85.4 | |
| 6 | 2.53 | 1.40 | 64.23 | -0.51 | 9.2 | 87.2 | |
| 7 | 1.40 | 0.27 | 64.61 | -0.51 | 11.8 | 85.2 | |
| 8 | 1.40 | 2.50 | 68.80 | -0.53 | 12.2 | 80.4 | |
| 9 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 10 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 11 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 12 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 13 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
中度 老化 | 1 | 0.60 | 0.60 | 56.53 | -0.70 | 9.2 | 82.9 |
| 2 | 1.80 | 0.60 | 56.29 | -0.86 | 6.5 | 62.0 | |
| 3 | 0.60 | 1.80 | 60.80 | -0.76 | 9.3 | 78.0 | |
| 4 | 1.80 | 1.80 | 58.80 | -0.99 | 6.6 | 60.1 | |
| 5 | 0.35 | 1.20 | 60.22 | -0.70 | 10.2 | 83.4 | |
| 6 | 2.05 | 1.20 | 57.63 | -0.65 | 7.5 | 69.2 | |
| 7 | 1.20 | 0.35 | 47.61 | -0.83 | 7.9 | 87.4 | |
| 8 | 1.20 | 2.05 | 62.89 | -0.79 | 8.5 | 70.2 | |
| 9 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 10 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 11 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 12 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 13 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
重度 老化 | 1 | 0.60 | 0.60 | 77.16 | -0.37 | 12.9 | 81.4 |
| 2 | 2.20 | 0.60 | 89.32 | -0.31 | 11.4 | 73.0 | |
| 3 | 0.60 | 2.20 | 77.86 | -0.40 | 13.9 | 81.9 | |
| 4 | 2.20 | 2.20 | 87.16 | -0.35 | 13.7 | 73.9 | |
| 5 | 0.27 | 1.40 | 78.54 | -0.36 | 14.1 | 81.7 | |
| 6 | 2.53 | 1.40 | 86.86 | -0.34 | 12.7 | 73.6 | |
| 7 | 1.40 | 0.27 | 83.45 | -0.30 | 11.9 | 75.6 | |
| 8 | 1.40 | 2.53 | 79.40 | -0.32 | 12.2 | 77.1 | |
| 9 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 10 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 11 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 12 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 13 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 |
| 种类 | 编号 | X3/% | X4/% | Y5/% | Y6/% | Y7/cm | Y8/0.1mm |
|---|---|---|---|---|---|---|---|
轻度 老化 | 1 | 0.60 | 0.60 | 66.49 | -0.47 | 12.0 | 82.9 |
| 2 | 2.20 | 0.60 | 62.66 | -0.49 | 9.2 | 81.6 | |
| 3 | 0.60 | 2.20 | 67.70 | -0.52 | 12.4 | 83.2 | |
| 4 | 2.20 | 2.20 | 61.44 | -0.52 | 10.1 | 81.7 | |
| 5 | 0.27 | 1.40 | 63.20 | -0.40 | 10.7 | 85.4 | |
| 6 | 2.53 | 1.40 | 64.23 | -0.51 | 9.2 | 87.2 | |
| 7 | 1.40 | 0.27 | 64.61 | -0.51 | 11.8 | 85.2 | |
| 8 | 1.40 | 2.50 | 68.80 | -0.53 | 12.2 | 80.4 | |
| 9 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 10 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 11 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 12 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
| 13 | 1.40 | 1.40 | 68.45 | -0.50 | 10.1 | 79.2 | |
中度 老化 | 1 | 0.60 | 0.60 | 56.53 | -0.70 | 9.2 | 82.9 |
| 2 | 1.80 | 0.60 | 56.29 | -0.86 | 6.5 | 62.0 | |
| 3 | 0.60 | 1.80 | 60.80 | -0.76 | 9.3 | 78.0 | |
| 4 | 1.80 | 1.80 | 58.80 | -0.99 | 6.6 | 60.1 | |
| 5 | 0.35 | 1.20 | 60.22 | -0.70 | 10.2 | 83.4 | |
| 6 | 2.05 | 1.20 | 57.63 | -0.65 | 7.5 | 69.2 | |
| 7 | 1.20 | 0.35 | 47.61 | -0.83 | 7.9 | 87.4 | |
| 8 | 1.20 | 2.05 | 62.89 | -0.79 | 8.5 | 70.2 | |
| 9 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 10 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 11 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 12 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
| 13 | 1.20 | 1.20 | 54.16 | -0.97 | 8.3 | 80.6 | |
重度 老化 | 1 | 0.60 | 0.60 | 77.16 | -0.37 | 12.9 | 81.4 |
| 2 | 2.20 | 0.60 | 89.32 | -0.31 | 11.4 | 73.0 | |
| 3 | 0.60 | 2.20 | 77.86 | -0.40 | 13.9 | 81.9 | |
| 4 | 2.20 | 2.20 | 87.16 | -0.35 | 13.7 | 73.9 | |
| 5 | 0.27 | 1.40 | 78.54 | -0.36 | 14.1 | 81.7 | |
| 6 | 2.53 | 1.40 | 86.86 | -0.34 | 12.7 | 73.6 | |
| 7 | 1.40 | 0.27 | 83.45 | -0.30 | 11.9 | 75.6 | |
| 8 | 1.40 | 2.53 | 79.40 | -0.32 | 12.2 | 77.1 | |
| 9 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 10 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 11 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 12 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 | |
| 13 | 1.40 | 1.40 | 79.57 | -0.30 | 10.3 | 76.0 |
| 响应指标 | 期望值 |
|---|---|
| 残留针入度比(25℃)/% | ≥57 |
| 质量损失/% | -0.80~0.80 |
| 延度(10℃)/cm | ≥6 |
| 针入度(25℃)/0.1mm | 80~100 |
| 响应指标 | 期望值 |
|---|---|
| 残留针入度比(25℃)/% | ≥57 |
| 质量损失/% | -0.80~0.80 |
| 延度(10℃)/cm | ≥6 |
| 针入度(25℃)/0.1mm | 80~100 |
| 再生剂类型 | 影响因子最优值 | 响应指标最优值 | ||||
|---|---|---|---|---|---|---|
| X3/% | X4/% | Y5/% | Y6/% | Y7/cm | Y8/0.1mm | |
| 轻度老化 | 0.60 | 1.02 | 66.13 | -0.45 | 11.1 | 83.0 |
| 中度老化 | 0.60 | 1.38 | 58.80 | -0.80 | 9.6 | 82.5 |
| 重度老化 | 0.62 | 0.90 | 77.77 | -0.35 | 12.6 | 80.2 |
| 再生剂类型 | 影响因子最优值 | 响应指标最优值 | ||||
|---|---|---|---|---|---|---|
| X3/% | X4/% | Y5/% | Y6/% | Y7/cm | Y8/0.1mm | |
| 轻度老化 | 0.60 | 1.02 | 66.13 | -0.45 | 11.1 | 83.0 |
| 中度老化 | 0.60 | 1.38 | 58.80 | -0.80 | 9.6 | 82.5 |
| 重度老化 | 0.62 | 0.90 | 77.77 | -0.35 | 12.6 | 80.2 |
| 再生剂种类 | 运动黏度(60℃)/mm2·s-1 | 闪点/℃ | 密度 (15℃)/g·cm-3 |
|---|---|---|---|
| 轻度老化再生剂 | 2570 | 237 | 1.00002 |
| 中度老化再生剂 | 2685 | 235 | 0.97077 |
| 重度老化再生剂 | 1710 | 267 | 0.98641 |
| 再生剂种类 | 运动黏度(60℃)/mm2·s-1 | 闪点/℃ | 密度 (15℃)/g·cm-3 |
|---|---|---|---|
| 轻度老化再生剂 | 2570 | 237 | 1.00002 |
| 中度老化再生剂 | 2685 | 235 | 0.97077 |
| 重度老化再生剂 | 1710 | 267 | 0.98641 |
| 沥青种类 | 针入度 (25℃)/0.01mm | 软化点/℃ | 延度 (10℃)/cm | 黏度 (135℃)/Pa·s |
|---|---|---|---|---|
| YS | 84.0 | 45.8 | 135.8 | 0.42 |
| RS | 55.2 | 50.8 | 9.6 | 0.59 |
| RS2 | 57.8 | 46.5 | 16.2 | 0.51 |
| RS4 | 63.5 | 45.6 | 35.1 | 0.48 |
| RS6 | 76.1 | 43.2 | 89.0 | 0.44 |
| RS8 | 86.0 | 41.8 | 113.0 | 0.42 |
| RS10 | 98.0 | 41.0 | 143.1 | 0.40 |
| MS | 43.9 | 49.6 | 4.4 | 0.77 |
| MS6 | 68.4 | 47.2 | 20.5 | 0.69 |
| MS8 | 79.5 | 45.4 | 29.4 | 0.61 |
| MS10 | 86.7 | 44.8 | 44.3 | 0.47 |
| MS12 | 93.5 | 42.4 | 52.8 | 0.42 |
| MS14 | 98.2 | 41.7 | 68.4 | 0.37 |
| PS | 25.9 | 60.7 | 1.2 | 1.05 |
| PS8 | 67.6 | 47.3 | 35.9 | 0.73 |
| PS10 | 78.8 | 44.4 | 41.1 | 0.52 |
| PS12 | 79.4 | 44.3 | 41.5 | 0.50 |
| PS14 | 85.2 | 43.1 | 46.2 | 0.47 |
| PS16 | 91.6 | 42.0 | 54.7 | 0.42 |
| 沥青种类 | 针入度 (25℃)/0.01mm | 软化点/℃ | 延度 (10℃)/cm | 黏度 (135℃)/Pa·s |
|---|---|---|---|---|
| YS | 84.0 | 45.8 | 135.8 | 0.42 |
| RS | 55.2 | 50.8 | 9.6 | 0.59 |
| RS2 | 57.8 | 46.5 | 16.2 | 0.51 |
| RS4 | 63.5 | 45.6 | 35.1 | 0.48 |
| RS6 | 76.1 | 43.2 | 89.0 | 0.44 |
| RS8 | 86.0 | 41.8 | 113.0 | 0.42 |
| RS10 | 98.0 | 41.0 | 143.1 | 0.40 |
| MS | 43.9 | 49.6 | 4.4 | 0.77 |
| MS6 | 68.4 | 47.2 | 20.5 | 0.69 |
| MS8 | 79.5 | 45.4 | 29.4 | 0.61 |
| MS10 | 86.7 | 44.8 | 44.3 | 0.47 |
| MS12 | 93.5 | 42.4 | 52.8 | 0.42 |
| MS14 | 98.2 | 41.7 | 68.4 | 0.37 |
| PS | 25.9 | 60.7 | 1.2 | 1.05 |
| PS8 | 67.6 | 47.3 | 35.9 | 0.73 |
| PS10 | 78.8 | 44.4 | 41.1 | 0.52 |
| PS12 | 79.4 | 44.3 | 41.5 | 0.50 |
| PS14 | 85.2 | 43.1 | 46.2 | 0.47 |
| PS16 | 91.6 | 42.0 | 54.7 | 0.42 |
| 样品种类 | 46℃ | 52℃ | 58℃ | 64℃ | 70℃ | |||||
|---|---|---|---|---|---|---|---|---|---|---|
| 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | |
| YS | 15.15 | 79.61 | 6.63 | 82.26 | 2.86 | 84.37 | 1.34 | 86.10 | 0.65 | 87.44 |
| RS | 32.29 | 77.15 | 11.26 | 80.26 | 5.23 | 82.76 | 2.29 | 84.85 | 1.09 | 86.51 |
| RS6 | 12.06 | 80.06 | 4.96 | 82.64 | 2.16 | 84.77 | 1.00 | 86.47 | 0.49 | 87.79 |
| MS | 35.23 | 76.09 | 13.94 | 79.29 | 5.73 | 82.06 | 2.49 | 84.29 | 1.14 | 86.04 |
| MS10 | 10.10 | 81.01 | 4.38 | 83.29 | 1.95 | 85.26 | 0.91 | 86.85 | 0.45 | 88.04 |
| PS | 121.80 | 67.05 | 47.57 | 70.75 | 18.61 | 74.40 | 8.97 | 77.86 | 4.17 | 81.01 |
| PS12 | 15.68 | 77.48 | 7.45 | 80.94 | 4.35 | 84.09 | 2.21 | 86.18 | 1.09 | 87.40 |
| 样品种类 | 46℃ | 52℃ | 58℃ | 64℃ | 70℃ | |||||
|---|---|---|---|---|---|---|---|---|---|---|
| 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | 复数剪切 模量/kPa | 相位角/(°) | |
| YS | 15.15 | 79.61 | 6.63 | 82.26 | 2.86 | 84.37 | 1.34 | 86.10 | 0.65 | 87.44 |
| RS | 32.29 | 77.15 | 11.26 | 80.26 | 5.23 | 82.76 | 2.29 | 84.85 | 1.09 | 86.51 |
| RS6 | 12.06 | 80.06 | 4.96 | 82.64 | 2.16 | 84.77 | 1.00 | 86.47 | 0.49 | 87.79 |
| MS | 35.23 | 76.09 | 13.94 | 79.29 | 5.73 | 82.06 | 2.49 | 84.29 | 1.14 | 86.04 |
| MS10 | 10.10 | 81.01 | 4.38 | 83.29 | 1.95 | 85.26 | 0.91 | 86.85 | 0.45 | 88.04 |
| PS | 121.80 | 67.05 | 47.57 | 70.75 | 18.61 | 74.40 | 8.97 | 77.86 | 4.17 | 81.01 |
| PS12 | 15.68 | 77.48 | 7.45 | 80.94 | 4.35 | 84.09 | 2.21 | 86.18 | 1.09 | 87.40 |
| 样品 种类 | 蠕变速率 | 蠕变劲度模量/MPa | ||||
|---|---|---|---|---|---|---|
| -12℃ | -18℃ | -24℃ | -12℃ | -18℃ | -24℃ | |
| YS | 0.418 | 0.361 | 0.265 | 87.5 | 214.0 | 552.0 |
| RS | 0.366 | 0.317 | 0.249 | 120.0 | 228.0 | 556.0 |
| RS6 | 0.497 | 0.409 | 0.315 | 46.1 | 136.0 | 392.0 |
| MS | 0.462 | 0.332 | 0.249 | 79.3 | 240.0 | 547.0 |
| MS10 | — | 0.411 | 0.304 | — | 104.0 | 319.0 |
| PS | 0.429 | 0.274 | 0.220 | 94.2 | 275.0 | 561.0 |
| PS12 | — | 0.405 | 0.345 | — | 92.7 | 234.0 |
| 样品 种类 | 蠕变速率 | 蠕变劲度模量/MPa | ||||
|---|---|---|---|---|---|---|
| -12℃ | -18℃ | -24℃ | -12℃ | -18℃ | -24℃ | |
| YS | 0.418 | 0.361 | 0.265 | 87.5 | 214.0 | 552.0 |
| RS | 0.366 | 0.317 | 0.249 | 120.0 | 228.0 | 556.0 |
| RS6 | 0.497 | 0.409 | 0.315 | 46.1 | 136.0 | 392.0 |
| MS | 0.462 | 0.332 | 0.249 | 79.3 | 240.0 | 547.0 |
| MS10 | — | 0.411 | 0.304 | — | 104.0 | 319.0 |
| PS | 0.429 | 0.274 | 0.220 | 94.2 | 275.0 | 561.0 |
| PS12 | — | 0.405 | 0.345 | — | 92.7 | 234.0 |
| 沥青种类 | 残留针入度比/% | 残留延度(10℃)/cm |
|---|---|---|
| RS6* | 56.28 | 7.3 |
| RS6 | 67.54 | 12.1 |
| MS10* | 58.52 | 4.8 |
| MS10 | 60.18 | 11.6 |
| PS12* | 75.56 | 1.1 |
| PS12 | 78.65 | 10.9 |
| 沥青种类 | 残留针入度比/% | 残留延度(10℃)/cm |
|---|---|---|
| RS6* | 56.28 | 7.3 |
| RS6 | 67.54 | 12.1 |
| MS10* | 58.52 | 4.8 |
| MS10 | 60.18 | 11.6 |
| PS12* | 75.56 | 1.1 |
| PS12 | 78.65 | 10.9 |
| 1 | WANG Fenglou LONG Jian, SHEN Benxian, et al. A study of the regenerating effects of recycling agents on aged asphalts[J]. Petroleum Science and Technology, 2014, 32(10): 1160-1167. |
| 2 | 李振海, 王国峰, 魏建明. 再生剂制备技术及再生沥青的评价[J]. 中国石油大学学报(自然科学版), 2011, 35(5): 152-156. |
| LI Zhenhai, WANG Guofeng, WEI Jianming. Preparation of recycling agent and evaluation on recycled asphalt[J]. Journal of China University of Petroleum (Edition of Natural Science), 2011, 35(5): 152-156. | |
| 3 | CHAFFIN Jay M, LIU Meng, DAVISON Richard R, et al. Supercritical fractions as asphalt recycling agents and preliminary aging studies on recycled asphalts[J]. Industrial & Engineering Chemistry Research, 1997, 36(3): 656-666. |
| 4 | 张鲁军, 赵庆民, 曲恒辉, 等. 沥青再生剂基础油分评价与再生机理研究[J]. 石油沥青, 2020, 34(4): 13-17. |
| ZHANG Lujun, ZHAO Qingmin, QU Henghui, et al. Study on the base oil evaluation and regeneration mechanism of asphalt regenerant[J]. Petroleum Asphalt, 2020, 34(4): 13-17. | |
| 5 | ZAUMANIS Martins, MALLICK Rajib B, POULIKAKOS Lily, et al. Influence of six rejuvenators on the performance properties of reclaimed asphalt pavement (RAP) binder and 100% recycled asphalt mixtures[J]. Construction and Building Materials, 2014, 71: 538-550. |
| 6 | 史柯, 马峰, 宋瑞萌, 等. 基于分子模拟的废大豆油再生沥青扩散行为[J]. 化工进展, 2024, 43(12):6794-6803. |
| SHI Ke, MA Feng, SONG Ruimeng, et al. Diffusion behavior of waste soybean oil rejuvenated bitumen based on molecular simulation[J]. Chemical Industry and Engineering Progress, 2024, 43(12): 6794-6803. | |
| 7 | 徐宁, 汪海年, 陈玉, 等. 餐饮废油对老化沥青的微观再生效应[J]. 铁道科学与工程学报, 2023, 20(9): 3406-3415. |
| XU Ning, WANG Hainian, CHEN Yu, et al. Microscopic regeneration effect of catering waste oil on aged asphalt[J]. Journal of Railway Science and Engineering, 2023, 20(9): 3406-3415. | |
| 8 | XU Huiping, WANG Fenglou, SHEN Benxian, et al. The synthesis and application of a new asphalt hot recycling agent[J]. Petroleum Science and Technology, 2014, 32(9): 1050-1057. |
| 9 | 谢泽华, 韦万峰. 高渗透性沥青再生剂的制备及其性能研究[J]. 西部交通科技, 2020(6): 12-15. |
| XIE Zehua, WEI Wanfeng. Study on preparation and properties of high permeability asphalt recycling agent[J]. Western China Communications Science & Technology, 2020(6): 12-15. | |
| 10 | 方四发, 张勇, 肖铭钊, 等. 具有改性功能的沥青再生剂的制备研究[J]. 建材世界, 2017, 38(4): 8-12. |
| FANG Sifa, ZHANG Yong, XIAO Mingzhao, et al. Research on the preparation of asphalt recycling agent with modified components[J]. The World of Building Materials, 2017, 38(4): 8-12. | |
| 11 | 况栋梁, 马小军, 马晓燕, 等. 废机油残留物再生剂对老化沥青动态力学性能和组分迁移的影响[J]. 材料导报, 2024, 38(2): 280-287. |
| KUANG Dongliang, MA Xiaojun, MA Xiaoyan, et al. Effect of waste oil residue regenerators on dynamic mechanical properties and component migration of aged asphalt[J]. Materials Reports, 2024, 38(2): 280-287. | |
| 12 | 万贵稳. 废食用油基沥青再生剂的制备与性能研究[D]. 武汉: 武汉理工大学, 2019. |
| WAN Guiwen. Preparation and properties of waste cooking oil-based asphalt rejuvenator[D]. Wuhan: Wuhan University of Technology, 2019. | |
| 13 | 孔令云, 席晗. 道路沥青紫外老化及抗老化材料研究综述[J]. 材料导报, 2024, 38(1): 48-60. |
| KONG Lingyun, XI Han. Review on ultraviolet aging and anti-aging materials of road asphalt[J]. Materials Reports, 2024, 38(1): 48-60. | |
| 14 | 罗浩原, 黄晓明. 废油再生沥青二次老化后的性能与组分变化[J]. 中国公路学报, 2021, 34(10): 98-110. |
| LUO Haoyuan, HUANG Xiaoming. Research on change of performance and component of recycled oil regenerated asphalt during secondary aging[J]. China Journal of Highway and Transport, 2021, 34(10): 98-110. | |
| 15 | 耿九光. 沥青老化机理及再生技术研究[D]. 西安: 长安大学, 2009. |
| GENG Jiuguang. Study on the aging mechanism and recycling technique of asphalt[D]. Xi’an: Changan University, 2009. | |
| 16 | LI Xudong, JIA Rong, LI Pingsheng, et al. Response surface analysis for enzymatic decolorization of Congo red by manganese peroxidase[J]. Journal of Molecular Catalysis B: Enzymatic, 2009, 56(1): 1-6. |
| 17 | 贺远鹏. 响应曲面法复配混凝剂处理海上生产返排液[J]. 化工进展, 2021, 40(S1): 439-445. |
| HE Yuanpeng. Treatment of offshore production flowback fluid with composite flocculant by response surface methodology[J]. Chemical Industry and Engineering Progress, 2021, 40(S1): 439-445. | |
| 18 | 鲁玉莹, 余黎明, 杨加可, 等. 响应面法优化制备LDHs-CRMA复合改性沥青及其表征[J]. 化工学报, 2020, 71(3): 1362-1369. |
| LU Yuying, YU Liming, YANG Jiake, et al. Preparation of LDHs-CRMA composite modified asphalt by response surface methodology and its characterization[J]. CIESC Journal, 2020, 71(3): 1362-1369. | |
| 19 | 臧超杰. 大掺量RAP厂拌热再生沥青混合料配合比优化设计与性能研究[D]. 兰州: 兰州理工大学, 2021. |
| ZANG Chaojie. Study on optimal design and performance of mixture ratio of hot recycled asphalt mixture with high volume RAP[D]. Lanzhou: Lanzhou University of Technology, 2021. | |
| 20 | 毛昱, 李萍, 念腾飞, 等. 再生剂在老化沥青中扩散行为的量化分析[J]. 华南理工大学学报(自然科学版), 2021, 49(2): 79-87. |
| MAO Yu, LI Ping, NIAN Tengfei, et al. Quantitative analysis of the diffusion behavior of rejuvenator in aged asphalt[J]. Journal of South China University of Technology (Natural Science Edition), 2021, 49(2): 79-87. | |
| 21 | 王俊生. 环保再生剂的制备及其对再生沥青及混合料性能的影响[D]. 重庆: 重庆交通大学, 2017. |
| WANG Junsheng. Preparation of environmental rejuvenator and its influence on performances of recycled bitumen and recycled asphalt mixture[D]. Chongqing: Chongqing Jiaotong University, 2017. | |
| 22 | 陈华鑫, 崔宇, 尹艳平, 等. 再生剂类型对沥青抗老化性能的影响[J]. 中国科技论文, 2022, 17(6): 589-594. |
| CHEN Huaxin, CUI Yu, YIN Yanping, et al. Influence of regeneration agent type on aging resistance properties of asphalt[J]. China Sciencepaper, 2022, 17(6): 589-594. | |
| 23 | 庄楚强, 何春雄. 应用数理统计基础[M]. 4版. 广州: 华南理工大学出版社, 2013. |
| ZHUANG Chuqiang, HE Chunxiong. Fundamentals of applied mathematical statistics[M]. 4th ed. Guangzhou: South China University of Technology Press, 2013. |
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