Chemical Industry and Engineering Progress ›› 2024, Vol. 43 ›› Issue (S1): 419-430.DOI: 10.16085/j.issn.1000-6613.2024-0620
• Materials science and technology • Previous Articles Next Articles
DU Xiaocong1,2(), XIN Chunfu1(), ZHAO Yu1,3
Received:
2024-04-12
Revised:
2024-07-02
Online:
2024-12-06
Published:
2024-11-20
Contact:
XIN Chunfu
通讯作者:
辛春福
作者简介:
杜小聪(1997—),男,硕士研究生,研究方向为绿色道路新材料研发与设计。E-mail:dxcsxht@163.com。
CLC Number:
DU Xiaocong, XIN Chunfu, ZHAO Yu. Performance evaluation of composite phase change materials and phase change modified asphalt for road use[J]. Chemical Industry and Engineering Progress, 2024, 43(S1): 419-430.
杜小聪, 辛春福, 赵钰. 路用复合相变材料及相变改性沥青性能评价[J]. 化工进展, 2024, 43(S1): 419-430.
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URL: https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2024-0620
名称 | 相变温度/℃ | 相变焓值 /J·g-1 | 参考文献 |
---|---|---|---|
低温聚氨酯相变材料 | -3.2 | 35.0 | [ |
聚乙二醇基聚氨酯(PU-5) | 48.3/36.0 | 93.5 | [ |
聚氨酯相变材料 | 43.9 | 146.6 | [ |
癸酸(CA) | 31.4 | 149.1 | [ |
肉豆蔻酸(MA) | 52.3 | 184.5 | [ |
硬脂酸(SA) | 67.2 | 199.1 | [ |
棕榈酸(PA) | 62.0 | 198.4 | [ |
月桂酸(LA) | 45.6 | 185.7 | [ |
聚乙二醇(PEG) | 54.0 | 112.3 | [ |
名称 | 相变温度/℃ | 相变焓值 /J·g-1 | 参考文献 |
---|---|---|---|
低温聚氨酯相变材料 | -3.2 | 35.0 | [ |
聚乙二醇基聚氨酯(PU-5) | 48.3/36.0 | 93.5 | [ |
聚氨酯相变材料 | 43.9 | 146.6 | [ |
癸酸(CA) | 31.4 | 149.1 | [ |
肉豆蔻酸(MA) | 52.3 | 184.5 | [ |
硬脂酸(SA) | 67.2 | 199.1 | [ |
棕榈酸(PA) | 62.0 | 198.4 | [ |
月桂酸(LA) | 45.6 | 185.7 | [ |
聚乙二醇(PEG) | 54.0 | 112.3 | [ |
载体类型 | 特点 | 名称 | 制备 方法 | 结论 | 参考 文献 |
---|---|---|---|---|---|
高分子 聚合物 | 具有不生锈、易于生产、导热性好、成本低且密度低等特点[ | 正十四烷/密胺树脂 | 原位聚合法 | 相变微胶囊具有良好的相变潜热和热稳定性,可用于沥青路面并进行研究 | [ |
正十四烷、二甲苯/环氧树脂 | 界面聚合法 | 随着芯材和载体质量比的增加,储热能力 增加,热裂解温度降低 | [ | ||
硬脂酸丁酯/聚脲、聚氨酯 | 界面聚合法 | 双层载体相比单层载体,致密性和稳定性 得到显著提高 | [ | ||
碳基材料 | 高导热性和良好的密度 | PA、SA/碳纳米管 | — | 碳纳米管能够降低熔融温度、提高凝固温度 | [ |
相变蜡/天然石墨改性聚乙烯 | — | 石墨的加入可以抵抗石蜡的软化作用 | [ | ||
黏土矿物 | 具有较高的热导率和良好的吸附性能,可以 很好地弥补液体PCMs渗漏的缺陷[ | PEG/多巴胺改性膨胀蛭石 | 真空浸渍法 | 多巴胺对增强CPCMs的封装率、熔化和 凝固过程中的潜热发挥着重要作用 | [ |
SA/三维蒙脱土骨架 | 真空浸渍法 | 具有显著的相变潜热和良好的传热能力,可实现太阳能的直接转化、储存和利用 | [ | ||
光催化 材料 | 热导率高、形状稳定、无腐蚀性等,制备的 温度及成本要求较高[ | 月桂酸/TiO2 | 溶胶-凝胶法 | 在200℃以内的高温环境下,CPCMs不会发生热分解且具有良好的热稳定性 | [ |
载体类型 | 特点 | 名称 | 制备 方法 | 结论 | 参考 文献 |
---|---|---|---|---|---|
高分子 聚合物 | 具有不生锈、易于生产、导热性好、成本低且密度低等特点[ | 正十四烷/密胺树脂 | 原位聚合法 | 相变微胶囊具有良好的相变潜热和热稳定性,可用于沥青路面并进行研究 | [ |
正十四烷、二甲苯/环氧树脂 | 界面聚合法 | 随着芯材和载体质量比的增加,储热能力 增加,热裂解温度降低 | [ | ||
硬脂酸丁酯/聚脲、聚氨酯 | 界面聚合法 | 双层载体相比单层载体,致密性和稳定性 得到显著提高 | [ | ||
碳基材料 | 高导热性和良好的密度 | PA、SA/碳纳米管 | — | 碳纳米管能够降低熔融温度、提高凝固温度 | [ |
相变蜡/天然石墨改性聚乙烯 | — | 石墨的加入可以抵抗石蜡的软化作用 | [ | ||
黏土矿物 | 具有较高的热导率和良好的吸附性能,可以 很好地弥补液体PCMs渗漏的缺陷[ | PEG/多巴胺改性膨胀蛭石 | 真空浸渍法 | 多巴胺对增强CPCMs的封装率、熔化和 凝固过程中的潜热发挥着重要作用 | [ |
SA/三维蒙脱土骨架 | 真空浸渍法 | 具有显著的相变潜热和良好的传热能力,可实现太阳能的直接转化、储存和利用 | [ | ||
光催化 材料 | 热导率高、形状稳定、无腐蚀性等,制备的 温度及成本要求较高[ | 月桂酸/TiO2 | 溶胶-凝胶法 | 在200℃以内的高温环境下,CPCMs不会发生热分解且具有良好的热稳定性 | [ |
制备方法 | 芯材 | 载体 | 相变温度 /℃ | 相变焓 /J·g-1 | 特点 | 参考 文献 |
---|---|---|---|---|---|---|
真空浸渍法 | 月桂酸 | 膨胀蛭石 | 41.88 | 126.8 | 主要通过毛细管力和表面张力进行吸附,能有效防泄漏 | [ |
相变石蜡 | 膨胀珍珠岩 | 24.52 | 88.31 | [ | ||
硬脂酸 棕榈酸 | 硅藻土 | 52.93 | 106.70 | [ | ||
熔融共混法 | 棕榈酸 硬脂酸 | 碳纳米管 | 53.95 | 177.70 | 适用于两种熔点相差较大的材料 | [ |
原位聚合法 | 十四烷 | 脲醛树脂 | -4.40 | 100.30 | 致密性好 性能可控 | [ |
十四烷 | 改性密胺树脂 | -4.08 | 140.60 | [ | ||
溶胶-凝胶法 | 聚乙二醇 | SiO2 | — | 113.80 | 操作简单、反应温度低、制备纯度高、成本高、易脆裂 | [ |
硬脂酸 | SiO2 | 54.90 | 90.30 | [ | ||
界面聚合法 | 硬脂酸丁酯 | 聚氨酯/聚脲双壁 | 24.10 | 85.00 | 操作简单、反应时间短,但利用成本低、制备成本高 | [ |
制备方法 | 芯材 | 载体 | 相变温度 /℃ | 相变焓 /J·g-1 | 特点 | 参考 文献 |
---|---|---|---|---|---|---|
真空浸渍法 | 月桂酸 | 膨胀蛭石 | 41.88 | 126.8 | 主要通过毛细管力和表面张力进行吸附,能有效防泄漏 | [ |
相变石蜡 | 膨胀珍珠岩 | 24.52 | 88.31 | [ | ||
硬脂酸 棕榈酸 | 硅藻土 | 52.93 | 106.70 | [ | ||
熔融共混法 | 棕榈酸 硬脂酸 | 碳纳米管 | 53.95 | 177.70 | 适用于两种熔点相差较大的材料 | [ |
原位聚合法 | 十四烷 | 脲醛树脂 | -4.40 | 100.30 | 致密性好 性能可控 | [ |
十四烷 | 改性密胺树脂 | -4.08 | 140.60 | [ | ||
溶胶-凝胶法 | 聚乙二醇 | SiO2 | — | 113.80 | 操作简单、反应温度低、制备纯度高、成本高、易脆裂 | [ |
硬脂酸 | SiO2 | 54.90 | 90.30 | [ | ||
界面聚合法 | 硬脂酸丁酯 | 聚氨酯/聚脲双壁 | 24.10 | 85.00 | 操作简单、反应时间短,但利用成本低、制备成本高 | [ |
性能名称 | 复合相变材料 | 评价指标 | 结论 | 参考文献 |
---|---|---|---|---|
高温性能 | 正十四烷/脲醛树脂 | 车辙因子 | 适当掺量的低温复合相变材料并不会影响沥青路面抵抗高温变形的路用性能 | [ |
聚乙二醇/膨胀石墨 | 车辙因子 | 复合相变材料的掺入提高了改性沥青混合料的抗车辙性能,但疲劳抗力受损且对沥青的低温性能不利 | [ | |
PEG/SiO2 | 动稳定度 | 使用PEG/SiO2相变颗粒替代矿粉,可有效提高沥青混合料的高温性能 | [ | |
粉煤灰载体CPCMs | 车辙深度 | 需要良好的磨耗层作为沥青的保护层,方能达到良好的抗车辙效果 | [ | |
低温性能 | 正十四烷/商用石墨烯改性密胺树脂 | 延度 | 通过商用石墨烯对密胺树脂进行改性可以提高沥青的低温性能 | [ |
正十四烷/白炭黑 | 弯拉应变 | 复合定形相变材料的掺加有利于提高沥青混合料的低温抗裂性,且沥青混合料的低温抗裂性随着复合定形相变材料掺量的增加而增强 | [ | |
正十四烷/硅粉 | 弯拉强度 弯拉应变 劲度模量 | 随着相变微胶囊掺量的增加,沥青混合料弯拉强度逐渐增大,弯拉应变减小,劲度模量增大 | [ | |
水稳定性 | NaCl/载体 | 劈裂强度 | 掺入相变材料作为填料的沥青混合料劈裂强度比矿粉高2.3%,抗冻融损坏能力强于普通 沥青混合料 | [ |
PEG/SiO2 | 残留稳定度 劈裂强度 | 掺入相变材料作为填料的沥青混合料劈裂强度、残留稳定度相比矿粉有所降低,对水稳定性的影响不大 | [ |
性能名称 | 复合相变材料 | 评价指标 | 结论 | 参考文献 |
---|---|---|---|---|
高温性能 | 正十四烷/脲醛树脂 | 车辙因子 | 适当掺量的低温复合相变材料并不会影响沥青路面抵抗高温变形的路用性能 | [ |
聚乙二醇/膨胀石墨 | 车辙因子 | 复合相变材料的掺入提高了改性沥青混合料的抗车辙性能,但疲劳抗力受损且对沥青的低温性能不利 | [ | |
PEG/SiO2 | 动稳定度 | 使用PEG/SiO2相变颗粒替代矿粉,可有效提高沥青混合料的高温性能 | [ | |
粉煤灰载体CPCMs | 车辙深度 | 需要良好的磨耗层作为沥青的保护层,方能达到良好的抗车辙效果 | [ | |
低温性能 | 正十四烷/商用石墨烯改性密胺树脂 | 延度 | 通过商用石墨烯对密胺树脂进行改性可以提高沥青的低温性能 | [ |
正十四烷/白炭黑 | 弯拉应变 | 复合定形相变材料的掺加有利于提高沥青混合料的低温抗裂性,且沥青混合料的低温抗裂性随着复合定形相变材料掺量的增加而增强 | [ | |
正十四烷/硅粉 | 弯拉强度 弯拉应变 劲度模量 | 随着相变微胶囊掺量的增加,沥青混合料弯拉强度逐渐增大,弯拉应变减小,劲度模量增大 | [ | |
水稳定性 | NaCl/载体 | 劈裂强度 | 掺入相变材料作为填料的沥青混合料劈裂强度比矿粉高2.3%,抗冻融损坏能力强于普通 沥青混合料 | [ |
PEG/SiO2 | 残留稳定度 劈裂强度 | 掺入相变材料作为填料的沥青混合料劈裂强度、残留稳定度相比矿粉有所降低,对水稳定性的影响不大 | [ |
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