Application of two-dimensional nanomaterials in pervaporation desalination membrane

doi:10.16085/j.issn.1000-6613.2022-0967

Abstract

Abstract:

Pervaporation (PV) possesses advantages such as the low requirement for feed water, high rejection and water recovery rate, and strong fouling resistance. Therefore, PV desalination can be competitive with other desalination technologies, especially for high-salinity brine. Current applications of PV desalination however are limited due to its relatively low separation efficiency, stability and fouling resistance. The introduction of novel membrane materials such as two-dimensional (2D) nanomaterials is considered to be an effective means to improve both the material properties and performance of PV desalination membranes. In this paper, a brief introduction to PV desalination technology is initially given. Then, the research status of two-dimensional nanomaterials in the field of PV desalination is reviewed from three perspectives: the properties and synthesis methods of nanomaterials, the preparation and modification strategies of nanocomposite membranes, and the influence of 2D nanomaterials on the properties and desalination performance of PV membranes. It is pointed out that the existing PV mass transfer model had great limitations and the synthesis of new two-dimensional nanomaterials faced great difficulty. To further improve the performance of PV compositemembranes and reduce the preparation cost, it is necessary to clarify the mass transfer mechanism of PV composite membrane and optimize the fabrication method of two-dimensional nanomaterials. In general, two-dimensional PV nanocomposite membranes with excellent separation performance and physicochemical properties will play an important role in the field of desalination.

Key words: pervaporation, 2D nanomaterials, desalination, membrane, composites

摘要：

渗透汽化（PV）具有预处理要求低，截留率及水回收率高、抗污染性强等优势，在水处理尤其是高盐废水处理方面具有巨大的应用前景。但目前PV脱盐技术的分离效率较低、稳定性差、抗污染性能欠佳的劣势限制了PV膜在分离膜技术的应用和认可。新型膜材料如二维纳米材料的引入使得PV膜从材料到性能都有了较大提升，被认为是提高PV膜脱盐性能的有效手段。本文首先介绍了PV脱盐技术的分离机理，并从3个方面综述了二维纳米材料在制备PV脱盐膜中的应用现状：二维纳米材料的分类与合成方法、PV复合脱盐膜的制备途径与稳定性提高策略以及二维纳米材料对PV膜特性及脱盐性能的影响。文中指出现有的PV传质模型存在较大局限性且新型二维纳米材料的合成方法较难，为了进一步提高PV复合膜的性能并降低制备成本，还需完善PV复合膜的传质机制并优化二维纳米材料的制备工艺。

关键词: 渗透汽化, 二维纳米材料, 脱盐, 膜, 复合材料

CLC Number:

TQ028.8

CHEN Yi, GUO Yaoli, YE Haixing, LI Yuxuan, NIU Q.Jason. Application of two-dimensional nanomaterials in pervaporation desalination membrane[J]. Chemical Industry and Engineering Progress, 2023, 42(3): 1437-1447.

陈仪, 郭耀励, 叶海星, 李宇璇, 牛青山. 二维纳米材料在渗透汽化脱盐膜中的应用[J]. 化工进展, 2023, 42(3): 1437-1447.

Figures/Tables 8

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PV脱盐膜	制备方法	NaCl浓度 /g·L^-1	实验条件	渗透通量 /L∙m^-2∙h^-1	截留率 /%	参考文献
GO/聚丙烯腈	真空抽滤法	3.5	90℃，真空0.1kPa	65.1	99.8	[21]
GO/多巴胺-α-氧化铝	真空抽滤法	3.5	90℃，真空	48.4	99.7	[24]
氧化石墨烯骨架（GOF）/对苯二异氰酸酯-α-氧化铝	真空抽滤法	3.5	90℃，真空	11.4	99.9	[52]
GO-聚乙烯醇/聚丙烯腈	真空抽滤法	3.5	70℃，真空0.1kPa	69.1	99.9	[28]
GO-聚乙烯醇/聚偏氟乙烯（PVDF）	溶液铸膜法	10	65℃，真空24kPa	28	99.9	[53]
GO-聚酰亚胺	相转化法	3.5	90℃，真空100kPa	36.1	99.9	[29]
GO-壳聚糖	溶液铸膜法	5	81℃，真空6kPa	30	99.9	[31]
GO-聚酰亚胺纤维	相转化法	3.5	90℃，真空100kPa	15.6	99.9	[30]
纳米石墨烯材料(GNPs)-聚醚嵌段酰胺/聚四氟乙烯	相转化法	马尔马拉海水	35℃，真空0.1kPa	2.5	99.8	[54]
GOF/多巴胺-α-氧化铝	真空抽滤法	3.5	90℃，真空	20.1	99.9	[55]
二胺分子交联 GO/多巴胺(PDA)-α-氧化铝	真空抽滤法	3.5	90℃，真空	19.7	99.9	[25]
GO/聚碳酸酯	抽滤涂层法	10	70℃，真空3kPa	42.4	99.9	[56]
GOF-磺基琥珀酸/尼龙底膜	真空抽滤法	3.5	70℃，真空0.13kPa	80.1	99.9	[23]
GO/聚丙烯中空纤维膜	真空抽滤法	3.321	70℃，真空	11.5	99.9	[33]
GO/海藻酸钠/聚甲基丙烯酸甲酯	溶液铸膜法	3	60℃，真空0.1kPa	8.11	99.41	[57]
GO-聚醚酰亚胺/聚酰胺	层层组装法	5	65℃，真空1.7kPa	13	99.9	[22]
GO-聚乙烯醇/混合纤维素膜	压力辅助抽滤法	10	85℃，真空6kPa	98	99.9	[58]
聚酰胺/GO/聚丙烯腈	压力辅助抽滤法	3.5	70℃，真空0.2kPa	26.7	99.9	[32]
阳离子交联-GO膜	真空抽滤法	纯水	20~25℃，真空2.8kPa	16.16	—	[27]
壳聚糖-氧化石墨烯(CGO)-二甲基苯磺酸/聚丙烯	压力辅助抽滤法	1.752	70℃，真空-95kPa	30.5	99.9	[34]
GO-Zn²⁺/聚醚砜	真空抽滤法	3	60℃，真空-100kPa	47.8	99.9	[26]
MXene/聚丙烯腈	真空抽滤法	3.5	65℃，真空0.4kPa	85.4	99.5	[41]
MXene-马来酸/尼龙底膜	真空抽滤法	3.5	65℃，真空0.1kPa	70	99	[43]
MXene-聚乙烯醇/聚四氟乙烯	溶液铸膜法	3.5	30℃，真空0.13kPa	62.2	99.8	[42]
ZSM-5/α-氧化铝	浸涂法	24	80℃，真空1kPa	6.4	99.5	[49]
AEL-聚酰胺/α-氧化铝	真空抽滤法	3.6	25℃，真空	3.3	99.9	[50]
ZSM-5/聚偏氟乙烯	真空抽滤法	22（混合盐）	73℃±2℃，真空	11	99.9	[51]

PV脱盐膜	制备方法	NaCl浓度 /g·L^-1	实验条件	渗透通量 /L∙m^-2∙h^-1	截留率 /%	参考文献
GO/聚丙烯腈	真空抽滤法	3.5	90℃，真空0.1kPa	65.1	99.8	[21]
GO/多巴胺-α-氧化铝	真空抽滤法	3.5	90℃，真空	48.4	99.7	[24]
氧化石墨烯骨架（GOF）/对苯二异氰酸酯-α-氧化铝	真空抽滤法	3.5	90℃，真空	11.4	99.9	[52]
GO-聚乙烯醇/聚丙烯腈	真空抽滤法	3.5	70℃，真空0.1kPa	69.1	99.9	[28]
GO-聚乙烯醇/聚偏氟乙烯（PVDF）	溶液铸膜法	10	65℃，真空24kPa	28	99.9	[53]
GO-聚酰亚胺	相转化法	3.5	90℃，真空100kPa	36.1	99.9	[29]
GO-壳聚糖	溶液铸膜法	5	81℃，真空6kPa	30	99.9	[31]
GO-聚酰亚胺纤维	相转化法	3.5	90℃，真空100kPa	15.6	99.9	[30]
纳米石墨烯材料(GNPs)-聚醚嵌段酰胺/聚四氟乙烯	相转化法	马尔马拉海水	35℃，真空0.1kPa	2.5	99.8	[54]
GOF/多巴胺-α-氧化铝	真空抽滤法	3.5	90℃，真空	20.1	99.9	[55]
二胺分子交联 GO/多巴胺(PDA)-α-氧化铝	真空抽滤法	3.5	90℃，真空	19.7	99.9	[25]
GO/聚碳酸酯	抽滤涂层法	10	70℃，真空3kPa	42.4	99.9	[56]
GOF-磺基琥珀酸/尼龙底膜	真空抽滤法	3.5	70℃，真空0.13kPa	80.1	99.9	[23]
GO/聚丙烯中空纤维膜	真空抽滤法	3.321	70℃，真空	11.5	99.9	[33]
GO/海藻酸钠/聚甲基丙烯酸甲酯	溶液铸膜法	3	60℃，真空0.1kPa	8.11	99.41	[57]
GO-聚醚酰亚胺/聚酰胺	层层组装法	5	65℃，真空1.7kPa	13	99.9	[22]
GO-聚乙烯醇/混合纤维素膜	压力辅助抽滤法	10	85℃，真空6kPa	98	99.9	[58]
聚酰胺/GO/聚丙烯腈	压力辅助抽滤法	3.5	70℃，真空0.2kPa	26.7	99.9	[32]
阳离子交联-GO膜	真空抽滤法	纯水	20~25℃，真空2.8kPa	16.16	—	[27]
壳聚糖-氧化石墨烯(CGO)-二甲基苯磺酸/聚丙烯	压力辅助抽滤法	1.752	70℃，真空-95kPa	30.5	99.9	[34]
GO-Zn²⁺/聚醚砜	真空抽滤法	3	60℃，真空-100kPa	47.8	99.9	[26]
MXene/聚丙烯腈	真空抽滤法	3.5	65℃，真空0.4kPa	85.4	99.5	[41]
MXene-马来酸/尼龙底膜	真空抽滤法	3.5	65℃，真空0.1kPa	70	99	[43]
MXene-聚乙烯醇/聚四氟乙烯	溶液铸膜法	3.5	30℃，真空0.13kPa	62.2	99.8	[42]
ZSM-5/α-氧化铝	浸涂法	24	80℃，真空1kPa	6.4	99.5	[49]
AEL-聚酰胺/α-氧化铝	真空抽滤法	3.6	25℃，真空	3.3	99.9	[50]
ZSM-5/聚偏氟乙烯	真空抽滤法	22（混合盐）	73℃±2℃，真空	11	99.9	[51]

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