Chemical Industry and Engineering Progress ›› 2023, Vol. 42 ›› Issue (2): 821-838.DOI: 10.16085/j.issn.1000-6613.2022-0702
• Materials science and technology • Previous Articles Next Articles
ZHANG Jianzhong1(), XU Sheng1,2(), FAN Jiashu1, FEI Zhenyu1, WANG Kun1, HUANG Jian1, CUI Fengbo1, RAN Wenhua1
Received:
2022-04-19
Revised:
2022-07-20
Online:
2023-03-13
Published:
2023-02-25
Contact:
XU Sheng
章建忠1(), 许升1,2(), 樊家澍1, 费振宇1, 王堃1, 黄建1, 崔峰波1, 冉文华1
通讯作者:
许升
作者简介:
章建忠(1981—),男,高级工程师,研究方向为高性能玻璃纤维产品的开发与应用。E-mail:jianzhong.zhang@jushi.com。
基金资助:
CLC Number:
ZHANG Jianzhong, XU Sheng, FAN Jiashu, FEI Zhenyu, WANG Kun, HUANG Jian, CUI Fengbo, RAN Wenhua. Progress in characterization and analysis of glass fiber sizing[J]. Chemical Industry and Engineering Progress, 2023, 42(2): 821-838.
章建忠, 许升, 樊家澍, 费振宇, 王堃, 黄建, 崔峰波, 冉文华. 玻璃纤维浸润剂的分析与表征技术进展[J]. 化工进展, 2023, 42(2): 821-838.
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URL: https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2022-0702
浸润剂表征技术 | 获得的浸润剂信息 |
---|---|
FTIR | 浸润剂组成的基本结构、浸润剂组分在玻璃纤维表面的吸附与黏结情况、硅烷层的水解情况、浸润剂的分解情况 |
NIR | 浸润剂中硅烷与成膜剂之间的反应 |
NMR | 鉴别玻璃纤维表面萃取的浸润剂结构与类型 |
GPC、HPLC | 萃取的浸润剂组分的分子量 |
IGC | 硅烷在玻璃纤维表面的吸附与结构、表面能、表面不均匀性(过于灵敏,无法给出浸润剂层的确切信息) |
LOI | 玻璃纤维表面浸润剂涂层的含量(无法给出浸润剂分布以及玻璃纤维与浸润剂间的作用信息) |
SIMS | 硅烷与成膜剂组分鉴别、复合材料的界面相形成、硅烷与成膜剂反应(需要二者中存在特定原子)、硅烷聚合程度 |
MDE | 浸润剂膜的溶胀作用(液态基体树脂渗透到浸润剂薄膜中的扩散系数以及浸润剂在基体树脂中的溶解性)、浸润剂与树脂间相互作用 |
GC/MS | 浸润剂热解产物鉴定 |
TGA | 浸润剂热稳定性、热降解行为(结果可能取决于浸润剂涂层的厚度) |
DSC、DMA | 浸润剂相转变温度及浸润剂、浸润剂对玻璃纤维-树脂界面相形成的影响、成膜剂的模量与热转变等 |
SEM | 浸润剂涂层形貌与涂覆效果 |
AFM | 浸润剂涂层表面形貌和粗糙度、硅烷层分布 (仅局部)、浸润剂与树脂界面相作用 |
EKA | 玻璃纤维表面的zeta电位、等电点、浸润剂组分优先吸附情况、纤维-树脂相互作用、硅烷在玻璃纤维表面的吸附情况 |
CA | 表面能、表面浸润剂涂层均匀性和厚度、润湿性、玻璃纤维表面羟基浓度 |
浸润剂表征技术 | 获得的浸润剂信息 |
---|---|
FTIR | 浸润剂组成的基本结构、浸润剂组分在玻璃纤维表面的吸附与黏结情况、硅烷层的水解情况、浸润剂的分解情况 |
NIR | 浸润剂中硅烷与成膜剂之间的反应 |
NMR | 鉴别玻璃纤维表面萃取的浸润剂结构与类型 |
GPC、HPLC | 萃取的浸润剂组分的分子量 |
IGC | 硅烷在玻璃纤维表面的吸附与结构、表面能、表面不均匀性(过于灵敏,无法给出浸润剂层的确切信息) |
LOI | 玻璃纤维表面浸润剂涂层的含量(无法给出浸润剂分布以及玻璃纤维与浸润剂间的作用信息) |
SIMS | 硅烷与成膜剂组分鉴别、复合材料的界面相形成、硅烷与成膜剂反应(需要二者中存在特定原子)、硅烷聚合程度 |
MDE | 浸润剂膜的溶胀作用(液态基体树脂渗透到浸润剂薄膜中的扩散系数以及浸润剂在基体树脂中的溶解性)、浸润剂与树脂间相互作用 |
GC/MS | 浸润剂热解产物鉴定 |
TGA | 浸润剂热稳定性、热降解行为(结果可能取决于浸润剂涂层的厚度) |
DSC、DMA | 浸润剂相转变温度及浸润剂、浸润剂对玻璃纤维-树脂界面相形成的影响、成膜剂的模量与热转变等 |
SEM | 浸润剂涂层形貌与涂覆效果 |
AFM | 浸润剂涂层表面形貌和粗糙度、硅烷层分布 (仅局部)、浸润剂与树脂界面相作用 |
EKA | 玻璃纤维表面的zeta电位、等电点、浸润剂组分优先吸附情况、纤维-树脂相互作用、硅烷在玻璃纤维表面的吸附情况 |
CA | 表面能、表面浸润剂涂层均匀性和厚度、润湿性、玻璃纤维表面羟基浓度 |
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