Chemical Industry and Engineering Progress ›› 2023, Vol. 42 ›› Issue (11): 5842-5851.DOI: 10.16085/j.issn.1000-6613.2022-2330
• Materials science and technology • Previous Articles
Received:
2022-12-18
Revised:
2023-01-13
Online:
2023-12-15
Published:
2023-11-20
Contact:
SUN Zhigao
通讯作者:
孙志高
作者简介:
黄志国(1994—),男,硕士研究生,研究方向为储能技术。E-mail:1178736316@qq.com。
基金资助:
CLC Number:
HUANG Zhiguo, SUN Zhigao. Preparation and properties of nano phase change microcapsules for heat storage[J]. Chemical Industry and Engineering Progress, 2023, 42(11): 5842-5851.
黄志国, 孙志高. 蓄热用纳米相变微胶囊制备与性能[J]. 化工进展, 2023, 42(11): 5842-5851.
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URL: https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2022-2330
名称 | 型号 | 精度 | 测量范围 |
---|---|---|---|
生物显微镜 | XSP-BM-3C | — | 40~1600倍 |
赛多利斯电子天平 | BSA224S | ±0.1mg | 0~220g |
数控超声波清洗器 | KQ100DE | — | RT+10~80℃ |
微电热恒温水槽 | THD-2015 | ±0.1℃ | -20~99℃ |
差示扫描量热仪 | NETZSCH DSC 200F3 | — | -180~725℃ |
傅里叶红外光谱仪 | Thermo Scientific Nicolet iS20 | — | 4000~400cm-1 |
真空干燥箱 | BZF-30 | ±0.5℃ | RT+2~250℃ |
扫描电子显微镜 | 蔡司Gemini300/Nova NanoSEM450 | — | — |
热导率测定仪 | DRE-Ⅲ | ≤3% | 0.005~50W/(m•K) |
名称 | 型号 | 精度 | 测量范围 |
---|---|---|---|
生物显微镜 | XSP-BM-3C | — | 40~1600倍 |
赛多利斯电子天平 | BSA224S | ±0.1mg | 0~220g |
数控超声波清洗器 | KQ100DE | — | RT+10~80℃ |
微电热恒温水槽 | THD-2015 | ±0.1℃ | -20~99℃ |
差示扫描量热仪 | NETZSCH DSC 200F3 | — | -180~725℃ |
傅里叶红外光谱仪 | Thermo Scientific Nicolet iS20 | — | 4000~400cm-1 |
真空干燥箱 | BZF-30 | ±0.5℃ | RT+2~250℃ |
扫描电子显微镜 | 蔡司Gemini300/Nova NanoSEM450 | — | — |
热导率测定仪 | DRE-Ⅲ | ≤3% | 0.005~50W/(m•K) |
样品 | 蒸馏水/mL | 无水乙醇/mL | SDS/g | HCl/mL | n-docosane/g | TBT/g |
---|---|---|---|---|---|---|
S1 | 72.0 | 36.0 | 0.5 | 0.10 | 5.0 | 5.0 |
S2 | 72.0 | 36.0 | 0.5 | 0.10 | 5.0 | 10.0 |
S3 | 72.0 | 36.0 | 0.5 | 0.25 | 5.0 | 5.0 |
S4 | 72.0 | 36.0 | 1.0 | 0.10 | 5.0 | 5.0 |
样品 | 蒸馏水/mL | 无水乙醇/mL | SDS/g | HCl/mL | n-docosane/g | TBT/g |
---|---|---|---|---|---|---|
S1 | 72.0 | 36.0 | 0.5 | 0.10 | 5.0 | 5.0 |
S2 | 72.0 | 36.0 | 0.5 | 0.10 | 5.0 | 10.0 |
S3 | 72.0 | 36.0 | 0.5 | 0.25 | 5.0 | 5.0 |
S4 | 72.0 | 36.0 | 1.0 | 0.10 | 5.0 | 5.0 |
材料 | 融化温度/℃ | 融化焓值/J·g-1 | 凝固温度/℃ | 凝固焓值/J·g-1 | 融化峰值温度/℃ | 凝固峰值温度/℃ | R/% | E/% | η/% |
---|---|---|---|---|---|---|---|---|---|
n-docosane | 42.9 | 251.6 | 42.7 | 254.15 | 45.7 | 40 | — | — | — |
TiO2@n-docosane | 41.3 | 178 | 42.4 | 171 | 44.7 | 35.4 | 70.7 | 69.0 | 97.6 |
材料 | 融化温度/℃ | 融化焓值/J·g-1 | 凝固温度/℃ | 凝固焓值/J·g-1 | 融化峰值温度/℃ | 凝固峰值温度/℃ | R/% | E/% | η/% |
---|---|---|---|---|---|---|---|---|---|
n-docosane | 42.9 | 251.6 | 42.7 | 254.15 | 45.7 | 40 | — | — | — |
TiO2@n-docosane | 41.3 | 178 | 42.4 | 171 | 44.7 | 35.4 | 70.7 | 69.0 | 97.6 |
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