Chemical Industry and Engineering Progress ›› 2019, Vol. 38 ›› Issue (06): 2825-2834.DOI: 10.16085/j.issn.1000-6613.2018-1935
• Materials science and technology • Previous Articles Next Articles
Qingjun GU(),Hua FEI(),Linya WANG,Min FANG,Dahua JIANG
Received:
2018-09-26
Online:
2019-06-05
Published:
2019-06-05
Contact:
Hua FEI
通讯作者:
费华
作者简介:
顾庆军(1993—),男,硕士研究生,研究方向为相变储能材料。E-mail:<email>gqj18896518935@163.com</email>。
基金资助:
CLC Number:
Qingjun GU, Hua FEI, Linya WANG, Min FANG, Dahua JIANG. Research progress on thermal properties of fatty acid phase change energy storage materials[J]. Chemical Industry and Engineering Progress, 2019, 38(06): 2825-2834.
顾庆军, 费华, 王林雅, 方敏, 蒋达华. 脂肪酸相变储能材料热性能研究进展[J]. 化工进展, 2019, 38(06): 2825-2834.
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相变材料 | 分子量 | 相变温度/℃ | 相变潜热 /J·g-1 | 热导率 /W·m-1·K-1 |
---|---|---|---|---|
CA | 172.27 | 30.10 | 152.00 | 0.153 |
LA | 200.32 | 43.00 | 177.00 | 0.147 |
MA | 228.37 | 53.70 | 187.00 | 0.150 |
PA | 256.42 | 62.30 | 186.00 | 0.162 |
SA | 284.48 | 70.70 | 203.00 | 0.172 |
相变材料 | 分子量 | 相变温度/℃ | 相变潜热 /J·g-1 | 热导率 /W·m-1·K-1 |
---|---|---|---|---|
CA | 172.27 | 30.10 | 152.00 | 0.153 |
LA | 200.32 | 43.00 | 177.00 | 0.147 |
MA | 228.37 | 53.70 | 187.00 | 0.150 |
PA | 256.42 | 62.30 | 186.00 | 0.162 |
SA | 284.48 | 70.70 | 203.00 | 0.172 |
单脂肪酸/ 脂肪醇 | 单脂肪酸/脂肪醇相变温度/℃ | 单脂肪酸/脂肪醇 相变焓值/J·g–1 | 二元脂肪酸醇 | 质量配比 | 二元脂肪酸醇 相变温度/℃ | 二元脂肪酸醇 相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
LA | 43.40 | 183.23 | LA-TD | 44∶56 | 24.46 | 150.45 | [ |
TD | 37.40 | 222.93 | |||||
DA | 6.0 | 205.7 | DA-PA | 97.8∶2.2 | 2.9 | 203.6 | [ |
PA | 62.1 | 210.2 | |||||
DA | 23.7 | 220.4 | DA-CA | 58.47∶41.53 | 8.9 | 159 | [ |
CA | 31.5 | 154 | |||||
LA | 44.40 | 181.50 | LA-LAL | 30∶70 | 26.50 | 101.22 | [ |
LAL | 23.10 | 242.15 | |||||
CA | 30.20 | 142.70 | CA-TD | 62∶38 | 19.13 | 153.40 | [ |
TD | 37.00 | 207.30 | LA-TD | 46.4∶53.6 | 24.40 | 162.70 | |
LA | 43.20 | 177.70 | MA-TD | 28.16∶71.84 | 34.45 | 208.00 | |
MA | 52.10 | 190.00 | |||||
CA | 15.42 | 150.99 | CA-LA | 70∶30 | 6.52 | 171.06 | [ |
LA | 22.84 | 207.30 |
单脂肪酸/ 脂肪醇 | 单脂肪酸/脂肪醇相变温度/℃ | 单脂肪酸/脂肪醇 相变焓值/J·g–1 | 二元脂肪酸醇 | 质量配比 | 二元脂肪酸醇 相变温度/℃ | 二元脂肪酸醇 相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
LA | 43.40 | 183.23 | LA-TD | 44∶56 | 24.46 | 150.45 | [ |
TD | 37.40 | 222.93 | |||||
DA | 6.0 | 205.7 | DA-PA | 97.8∶2.2 | 2.9 | 203.6 | [ |
PA | 62.1 | 210.2 | |||||
DA | 23.7 | 220.4 | DA-CA | 58.47∶41.53 | 8.9 | 159 | [ |
CA | 31.5 | 154 | |||||
LA | 44.40 | 181.50 | LA-LAL | 30∶70 | 26.50 | 101.22 | [ |
LAL | 23.10 | 242.15 | |||||
CA | 30.20 | 142.70 | CA-TD | 62∶38 | 19.13 | 153.40 | [ |
TD | 37.00 | 207.30 | LA-TD | 46.4∶53.6 | 24.40 | 162.70 | |
LA | 43.20 | 177.70 | MA-TD | 28.16∶71.84 | 34.45 | 208.00 | |
MA | 52.10 | 190.00 | |||||
CA | 15.42 | 150.99 | CA-LA | 70∶30 | 6.52 | 171.06 | [ |
LA | 22.84 | 207.30 |
单脂肪酸 | 单脂肪酸 相变温度/℃ | 单脂肪酸 相变焓值/J·g–1 | 二元或多元脂肪酸 | 质量配比 | 二元或多元脂酸相变温度/℃ | 二元或多元脂肪酸 相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
CA | 32.14 | 156.40 | CA-PA | 85:15 | 27.48 | 151.54 | [ |
PA | 58.90 | 189.60 | |||||
CA | 32.14 | 156.40 | CA-MA | 74:26 | 22.61 | 154.83 | [ |
MA | 53.86 | 190.00 | |||||
CA | 16 | 146.45 | CA-MA | 87:13 | 7.13 | 146.1 | [ |
MA | 52.2 | 182.6 | |||||
CA | 31.49 | 150.80 | CA-LA | 62:38 | 18.63 | 121.00 | [ |
LA | 43.53 | 172.60 | |||||
CA | 31.00 | 154.90 | CA-SA | 90:10 | 26.8 | 96.4 | [ |
SA | 67.53 | 211.60 | |||||
CA | 30.30 | 152.10 | CA-LA-PA | 50:30:20 | 16.80 | 140.50 | [ |
LA | 42.80 | 180.20 | |||||
PA | 61.40 | 220.70 | |||||
LA | 44.00 | 174.90 | LA-PA-SA | 62.2:24.6:13.2 | 32.10 | 151.60 | [ |
PA | 62.00 | 198.40 | |||||
SA | 68.50 | 201.80 |
单脂肪酸 | 单脂肪酸 相变温度/℃ | 单脂肪酸 相变焓值/J·g–1 | 二元或多元脂肪酸 | 质量配比 | 二元或多元脂酸相变温度/℃ | 二元或多元脂肪酸 相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
CA | 32.14 | 156.40 | CA-PA | 85:15 | 27.48 | 151.54 | [ |
PA | 58.90 | 189.60 | |||||
CA | 32.14 | 156.40 | CA-MA | 74:26 | 22.61 | 154.83 | [ |
MA | 53.86 | 190.00 | |||||
CA | 16 | 146.45 | CA-MA | 87:13 | 7.13 | 146.1 | [ |
MA | 52.2 | 182.6 | |||||
CA | 31.49 | 150.80 | CA-LA | 62:38 | 18.63 | 121.00 | [ |
LA | 43.53 | 172.60 | |||||
CA | 31.00 | 154.90 | CA-SA | 90:10 | 26.8 | 96.4 | [ |
SA | 67.53 | 211.60 | |||||
CA | 30.30 | 152.10 | CA-LA-PA | 50:30:20 | 16.80 | 140.50 | [ |
LA | 42.80 | 180.20 | |||||
PA | 61.40 | 220.70 | |||||
LA | 44.00 | 174.90 | LA-PA-SA | 62.2:24.6:13.2 | 32.10 | 151.60 | [ |
PA | 62.00 | 198.40 | |||||
SA | 68.50 | 201.80 |
单脂肪酸/石蜡 | 单脂肪酸/石蜡相变温度/℃ | 单脂肪酸/石蜡 相变焓值/J·g–1 | 脂肪酸-石蜡 二元混合物 | 质量配比 | 脂肪酸-石蜡二元 混合物相变温度/℃ | 脂肪酸-石蜡二元混合物相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
CA | 28.5 | 145.5 | CA-PW | 80∶20 | 25.5 | 144.7 | [ |
PW | 52 | 250 | |||||
PA | 62.98 | 236.18 | PA-PW | 15∶85 | 44.5 | 210.5 | [ |
PW | 52.76 | 220.52 | |||||
SA | 56 | 177.6 | SA-PW | 50∶50 | 50.62 | 171.9 | [ |
PW | 52.5 | 169.7 |
单脂肪酸/石蜡 | 单脂肪酸/石蜡相变温度/℃ | 单脂肪酸/石蜡 相变焓值/J·g–1 | 脂肪酸-石蜡 二元混合物 | 质量配比 | 脂肪酸-石蜡二元 混合物相变温度/℃ | 脂肪酸-石蜡二元混合物相变焓值/J·g–1 | 文献及年份 |
---|---|---|---|---|---|---|---|
CA | 28.5 | 145.5 | CA-PW | 80∶20 | 25.5 | 144.7 | [ |
PW | 52 | 250 | |||||
PA | 62.98 | 236.18 | PA-PW | 15∶85 | 44.5 | 210.5 | [ |
PW | 52.76 | 220.52 | |||||
SA | 56 | 177.6 | SA-PW | 50∶50 | 50.62 | 171.9 | [ |
PW | 52.5 | 169.7 |
相变材料 | 多孔基材 | 质量配比 | 作用 | 参考文献 |
---|---|---|---|---|
CA-LA | Dm | 85∶15 | 热导率从0.22W·m-1·K-1增加到0.47W·m-1·K-1 | [ |
CA | Bn | 40∶60 | 热导率从0.18W·m-1·K-1增加到0.43W·m-1·K-1 | [ |
CA | Kl | 17.5∶82.5 | 热导率从0.18W·m-1·K-1增加到0.23W·m-1·K-1 | [ |
CA-LA-PA | EG | 95∶5 | 热导率增加到0.738W·m-1·K-1,约是原材料的4.5倍 | [ |
LA-PA-SA | EG | 93.75∶6.25 | 融化时间减少了85%,凝固时间减少了83.3% | [ |
SA-AC | EG | 90∶10 | 热导率从0.336W·m-1·K-1增加到5.909W·m-1·K-1 | [ |
相变材料 | 多孔基材 | 质量配比 | 作用 | 参考文献 |
---|---|---|---|---|
CA-LA | Dm | 85∶15 | 热导率从0.22W·m-1·K-1增加到0.47W·m-1·K-1 | [ |
CA | Bn | 40∶60 | 热导率从0.18W·m-1·K-1增加到0.43W·m-1·K-1 | [ |
CA | Kl | 17.5∶82.5 | 热导率从0.18W·m-1·K-1增加到0.23W·m-1·K-1 | [ |
CA-LA-PA | EG | 95∶5 | 热导率增加到0.738W·m-1·K-1,约是原材料的4.5倍 | [ |
LA-PA-SA | EG | 93.75∶6.25 | 融化时间减少了85%,凝固时间减少了83.3% | [ |
SA-AC | EG | 90∶10 | 热导率从0.336W·m-1·K-1增加到5.909W·m-1·K-1 | [ |
相变材料 | 多孔基材 | 质量配比 | 作用 | 参考文献 |
---|---|---|---|---|
SA | Gr | 95∶5 | 热导率最大提高了63.4% | [ |
SA | Gr | 95∶5 | 热导率提高了71.7% | [ |
SA | TiO2 | 30.36∶69.64 | 热导率最大提高了2.5倍 | [ |
PA | SiO2 | 83.25∶16.75 | 热导率从0.21W·m-1·K-1增加到0.71W·m-1·K-1 | [ |
PA | AlOOH | 52∶48 | 热导率从0.16W·m-1·K-1增加到0.84W·m-1·K-1 | [ |
相变材料 | 多孔基材 | 质量配比 | 作用 | 参考文献 |
---|---|---|---|---|
SA | Gr | 95∶5 | 热导率最大提高了63.4% | [ |
SA | Gr | 95∶5 | 热导率提高了71.7% | [ |
SA | TiO2 | 30.36∶69.64 | 热导率最大提高了2.5倍 | [ |
PA | SiO2 | 83.25∶16.75 | 热导率从0.21W·m-1·K-1增加到0.71W·m-1·K-1 | [ |
PA | AlOOH | 52∶48 | 热导率从0.16W·m-1·K-1增加到0.84W·m-1·K-1 | [ |
相变材料 | 质量配比 | 高导材料 | 添加量 | 作用 | 参考文献 |
---|---|---|---|---|---|
MA | — | Gr | 0.5%,1%,2% | 热导率分别增加了6.7%,20%,40% | [ |
CA-MA/VMT | 20:80 | EG | 2% | 热导率从0.12W·m-1·K-1增加到0.22W·m-1·K-1 | [ |
LA-PA-SA/EP | 55:45 | EG | 2% | 热导率提高了95% | [ |
CA-MA/PMMA | 72:28 | MG | 2%,5%,7%,10%,15% | 热导率分别增加了10.8%,33.4%,46%,59.5%,89% | [ |
PA-SA/Bn | 50:50 | EG | 4% | 热导率提高了5.6倍 | [ |
SF/CA-PA | 68:32 | CNT | 1%,3%,5% | 热导率分别增加了12.9%,32.3%,56.1% | [ |
SA | — | CNT | 0.1% | 热导率提高了8.3% | [ |
SA | — | CNT | 40% | 热导率提高了27.9倍 | [ |
SA | — | CNT | 0.1%,0.5%,1%,3% | 热导率分别增加了4.6%,6.3%,8.6%,11.4% | [ |
PA | — | CNT | 1% | 热导率提高了35% | [ |
MA-SA | 54:46 | CNT | 9%,12%,15% | 热导率分别增加了23.2%,49.4%,63.7% | [ |
MA/HDPE | 70:30 | Al2O3 | 4%,8%,12% | 热导率分别增加了38.7%,71%,94.6% | [ |
LA-MA-SA/aEV | 57.7:42.3 | Al2O3 | 12% | 热导率提高了37.5% | [ |
DA-CA | 58.47:41.53 | Al2O3 | 0.1g·L-1 | 热导率提高了14.9% | [ |
Cu | 0.1g·L-1 | 热导率提高了8.5% | |||
CA-PA | 79:21 | Al2O3 | 20% | 热导率从0.3038W·m-1·K-1增加到0.5051W·m-1·K-1 | [ |
CA-CA | 30:70 | Cu | 0.1%,0.2%,0.3%,0.4% | 热导率分别增加了5.1%,5.8%,6.2%,6.6% | [ |
Al2O3 | 0.1%,0.2%,0.3%,0.4% | 热导率分别增加了4%,8%,11%,13% | |||
Fe2O3 | 0.1%,0.2%,0.3% | 热导率分别增加了6.6%,9.5%,17.5% | |||
PA-LA | 80:20 | Ss | — | 几乎没影响 | [ |
SA-MA | 80:20 | Cu | — | 融化时间减少了22%,凝固时间减少了61% | |
Gr | — | 融化时间减少了54%,凝固时间减少了71% | |||
Ss | — | 几乎没影响 | |||
Cu | — | 融化时间减少了33%,凝固时间减少了65% | |||
Gr | — | 融化时间减少了33%,凝固时间减少了50% |
相变材料 | 质量配比 | 高导材料 | 添加量 | 作用 | 参考文献 |
---|---|---|---|---|---|
MA | — | Gr | 0.5%,1%,2% | 热导率分别增加了6.7%,20%,40% | [ |
CA-MA/VMT | 20:80 | EG | 2% | 热导率从0.12W·m-1·K-1增加到0.22W·m-1·K-1 | [ |
LA-PA-SA/EP | 55:45 | EG | 2% | 热导率提高了95% | [ |
CA-MA/PMMA | 72:28 | MG | 2%,5%,7%,10%,15% | 热导率分别增加了10.8%,33.4%,46%,59.5%,89% | [ |
PA-SA/Bn | 50:50 | EG | 4% | 热导率提高了5.6倍 | [ |
SF/CA-PA | 68:32 | CNT | 1%,3%,5% | 热导率分别增加了12.9%,32.3%,56.1% | [ |
SA | — | CNT | 0.1% | 热导率提高了8.3% | [ |
SA | — | CNT | 40% | 热导率提高了27.9倍 | [ |
SA | — | CNT | 0.1%,0.5%,1%,3% | 热导率分别增加了4.6%,6.3%,8.6%,11.4% | [ |
PA | — | CNT | 1% | 热导率提高了35% | [ |
MA-SA | 54:46 | CNT | 9%,12%,15% | 热导率分别增加了23.2%,49.4%,63.7% | [ |
MA/HDPE | 70:30 | Al2O3 | 4%,8%,12% | 热导率分别增加了38.7%,71%,94.6% | [ |
LA-MA-SA/aEV | 57.7:42.3 | Al2O3 | 12% | 热导率提高了37.5% | [ |
DA-CA | 58.47:41.53 | Al2O3 | 0.1g·L-1 | 热导率提高了14.9% | [ |
Cu | 0.1g·L-1 | 热导率提高了8.5% | |||
CA-PA | 79:21 | Al2O3 | 20% | 热导率从0.3038W·m-1·K-1增加到0.5051W·m-1·K-1 | [ |
CA-CA | 30:70 | Cu | 0.1%,0.2%,0.3%,0.4% | 热导率分别增加了5.1%,5.8%,6.2%,6.6% | [ |
Al2O3 | 0.1%,0.2%,0.3%,0.4% | 热导率分别增加了4%,8%,11%,13% | |||
Fe2O3 | 0.1%,0.2%,0.3% | 热导率分别增加了6.6%,9.5%,17.5% | |||
PA-LA | 80:20 | Ss | — | 几乎没影响 | [ |
SA-MA | 80:20 | Cu | — | 融化时间减少了22%,凝固时间减少了61% | |
Gr | — | 融化时间减少了54%,凝固时间减少了71% | |||
Ss | — | 几乎没影响 | |||
Cu | — | 融化时间减少了33%,凝固时间减少了65% | |||
Gr | — | 融化时间减少了33%,凝固时间减少了50% |
方法 | 增强材料 | 优点 | 缺点 |
---|---|---|---|
多孔基材吸附 | 硅藻土、膨润土、高岭土、 | 吸附过程简单,导热增强效果 | 成本较高,降低复合材料的相变潜热 |
膨胀石墨等 | 明显,抑制液相泄漏 | ||
微胶囊化 | 二氧化硅、二氧化钛、碳酸钙、氧化铝等 | 直接加工成型,使用安全方便, | 成本高,制备工艺复杂,易磨损破裂, |
提高导热性能,抑制液相泄漏 | 降低复合材料的相变潜热 | ||
添加高导热材料 | 石墨、碳纳米管、金属、 | 操作简单易实现,成本较低,改善导热性能 | 降低复合材料的潜热 |
石墨烯等 |
方法 | 增强材料 | 优点 | 缺点 |
---|---|---|---|
多孔基材吸附 | 硅藻土、膨润土、高岭土、 | 吸附过程简单,导热增强效果 | 成本较高,降低复合材料的相变潜热 |
膨胀石墨等 | 明显,抑制液相泄漏 | ||
微胶囊化 | 二氧化硅、二氧化钛、碳酸钙、氧化铝等 | 直接加工成型,使用安全方便, | 成本高,制备工艺复杂,易磨损破裂, |
提高导热性能,抑制液相泄漏 | 降低复合材料的相变潜热 | ||
添加高导热材料 | 石墨、碳纳米管、金属、 | 操作简单易实现,成本较低,改善导热性能 | 降低复合材料的潜热 |
石墨烯等 |
添加剂 | 优点 | 缺点 |
---|---|---|
石墨 | 导热增强效果最显著,抑制液相泄漏 | 降低复合材料的相变潜热 |
碳纳米管 | 导热增强效果较显著,抑制液相泄漏 | 酸化等处理过程复杂,成本较高,降低相变材料的潜热值及 |
液相自然对流作用 | ||
金属 | 改善导热性能,过程简单,成本低, | 有可能减小复合材料的相变潜热 |
有可能提高复合材料的相变潜热 |
添加剂 | 优点 | 缺点 |
---|---|---|
石墨 | 导热增强效果最显著,抑制液相泄漏 | 降低复合材料的相变潜热 |
碳纳米管 | 导热增强效果较显著,抑制液相泄漏 | 酸化等处理过程复杂,成本较高,降低相变材料的潜热值及 |
液相自然对流作用 | ||
金属 | 改善导热性能,过程简单,成本低, | 有可能减小复合材料的相变潜热 |
有可能提高复合材料的相变潜热 |
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