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超声波-机械搅拌联合乳化重油分散度实验

李 博1,王 华1,朱道飞1,胡建杭1,王 冲2,熊振昆2   

  1. 1 昆明理工大学冶金与能源工程学院;2 广东清远云铜有色金属有限公司
  • 出版日期:2010-06-05 发布日期:2010-06-05

Dispersity of emulsified heavy-oil under combined ultrasonic
and mechanical stirring

LI Bo1,WANG Hua1,ZHU Daofei1,HU Jianhang1,WANG Chong2,XIONG Zhenkun2   

  1. 1 Faculty of Metallurgy and Energy Engineering,Kunming University of Science and Technology;2 Yunnan Copper Group Guangdong Qingyuan
    Non-ferrous Metal Co. Ltd.
  • Online:2010-06-05 Published:2010-06-05

摘要: 采用超声波-机械搅拌联合乳化(联合法)重油技术,根据索太尔平均直径(SMD)计算法,研究了超声功率、超声频率、乳化温度、乳化时间对乳化重油中分散相(水)分散度的影响,并比较了以上因素对超声波法与联合法乳化重油分散度影响的差别。结果表明:联合法乳化重油的分散度高于超声波法,分散相(水)的SMD降低4~8 mm;超声功率、乳化温度的增加有利于分散度的提高,但乳化温度不宜超过90 ℃;较低的超声频率有利于水在重油中的微细化;随着乳化时间的增加,乳化重油分散度先提高后降低。本实验得出联合法乳化重油的理想工艺条件为:超声功率为500~600 W,超声频率为25~40 kHz,乳化温度为70~80 ℃,乳化时间为30 min左右。

Abstract: A combined emulsification technique was introduced to intensify emulsification by means of ultrasonic and mechanical stirring. Effects of ultrasonic power,ultrasonic frequency,emulsification temperature and time on the dispersity of water in heavy-oil by the combined technique or ultrasonic stirring alone were investigated on the basis of Sauter mean diameter(SMD)calculation. Results showed that the combined technique could achieve a higher dispersity of water with a 4—8 μm decrease in SMD of the disperse phase. The dispersity of water increases with the increase in ultrasonic power and emulsification temperature,while the emulsification temperature should not be higher than 90 ℃. Lower ultrasonic frequencies are favorable to the micronization of water in heavy oil. With the increase in emulsification time,the dispersity of water first increase and then decrease. As a result,the optimal experimental conditions can be considered as is 500—600 W of ultrasonic power,25—40 kHz of ultrasonic frequency,70—80 ℃ of emulsification temperature,and about 30min of emulsification time.

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