化工进展

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漂白紫胶脱水除盐工艺

于连松1,2,张 弘1,周梅村2,郑 华1,陈晓鸣1,甘 瑾1   

  1. 1中国林业科学研究院资源昆虫研究所,云南 昆明 650224;2昆明理工大学化学工程学院,云南 昆明 650224
  • 出版日期:2010-10-05 发布日期:2010-10-05

Dehydration and desalination process of bleached shellac

YU Liansong1,2,ZHANG Hong1,ZHOU Meicun2,ZHENG Hua1,CHEN Xiaoming1,GAN Jin1   

  1. 1 Research Institute of Resource Insects,Chinese Academy of Forestry,Kunming 650224,Yunnan,China;2 Faculty of Chemical Engineering,Kunming University of Science and Technology,Kunming 650224,Yunnan,China
  • Online:2010-10-05 Published:2010-10-05

摘要:

为减轻后续工艺的生产压力、提高生产效率,研究了在漂白紫胶水洗脱盐的同时脱水的工艺条件。为得到漂白紫胶脱水除盐工艺的优化条件,研究了不同水洗温度和水洗时间条件下漂白紫胶产品的脱水率、颜色指数和水溶物,用响应曲面法(RSM)设计试验并建立了该工艺条件的拟合方程。试验结果表明,拟合方程的拟合度较高,所建立的数学模型可以用于描述漂白紫胶的脱水除盐工艺。通过优化得到了漂白紫胶脱水除盐工艺的最优条件:温度为33 ℃、水洗时间为11 min,可以得到脱水率为69.29%、颜色指数为1.0、水溶物为0.3969%的产品。

Abstract:

The dehydration process conditions of bleached shellac while desalination washing was investigated by experimental design with response surface methodRSM. The dehydration ratecolor index and the water-solubles in product were determined under different washing time and temperaturethrough which a fitting equation of the process was established. Results showed that the equation was well fittedand the established mathematical model could be used to describe the dehydration and desalination process of bleached shellac. The optimal dehydration and desalination process conditions were found at 33 for 11 min washingunder whichproducts were obtained with dehydration rate of 69.29%color index of 1.0 and water-solubles of 0.3969%.

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