CAI LianguoXU YongquanCHEN JianfengSHAO Lei" /> NaY分子筛合成工艺

化工进展

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NaY分子筛合成工艺

蔡连国,许永权,陈建峰,邵 磊   

  1. 北京化工大学纳米材料先进制备技术与应用科学教育部重点实验室
  • 出版日期:2006-12-25 发布日期:2006-12-25

Synthesis of NaY molecular sieve

CAI LianguoXU YongquanCHEN JianfengSHAO Lei   

  1. Key Lab for Nanomaterials, Ministry of Education, Beijing University of Chemical Technology
  • Online:2006-12-25 Published:2006-12-25

摘要: 报道了以具有独特组成的硅铝凝胶为导向剂制备NaY分子筛的方法。所合成的NaY分子筛用SEMXRDBET等进行了表征,结果表明,该NaY分子筛粒径2 μm左右,硅铝比n(SiO2)/n(Al2O3)3.28,结晶度90%,比表面积703 m2/g。除晶化过程外,该合成NaY分子筛的工艺过程均在室温下进行,具有反应条件温和,易于调控的特点。

Abstract: A novel method for the preparation of NaY molecular sieve by using a Si-Al gel with special composition as the directing agent was presented. The as-synthesized NaY molecular sieve was characterized with SEM, XRD and BET. The NaY molecular sieve had a particle size of approximately 2μm, n(SiO2)/n(Al2O3) of 3.28, crystallinity of 90% and specific surface area of 703 m2/g. Except the crystallization process, the synthesis of the NaY molecular sieve was conducted at room temperature under mild and controllable reaction conditions.

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