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Study on the preparation of impregnating pitch by solvent-sedimentation method

MA Wenming1,2,XIONG Jieming2,CHI Yaoling2,GE Minglan2,JIA Zhongbao1,PENG Xiaoxi1   

  1. 1College of Chemical Engineering,Beijing University of chemical Technology,Beijing 100029,China; 2 College of Chemical Engineering,Beijing Institutes of Petrochemical Technology,Beijing 102617,China
  • Online:2013-03-05 Published:2013-03-05

溶剂沉降法制备浸渍剂沥青

马文明1,2,熊杰明2,迟姚玲2,葛明兰2,贾中宝1,彭晓希1   

  1. 1北京化工大学化学工程学院,北京 100029;2北京石油化工学院化学工程学院,北京 102617

Abstract: Impregnating pitch is a densified reinforcing agent for improving carbon products. Quinoline insoluble matter (QI) in raw coal pitch is removed by solvent-sedimentation method,and then the solvent was removed by distillation under reduced pressure to obtain the impregnating pitch products. The operating conditions of the removal of quinoline insoluble are discussed,including the ratio of solvent,settling temperature,distillation temperature. The comparison of the performance of impregnated asphalt products prepared by the different raw materials are conducted. Impregnating pitch products with 83 ℃ of softening point,0.084% of quinoline insoluble and 49.32% of coking value were obtained.

Key words: coal tar pitch, solvent-sedimentation method, impregnating pitch

摘要: 通过溶剂沉降法脱除各种原料煤沥青中的喹啉不溶物(QI),再用减压蒸馏去除溶剂,得到浸渍剂沥青产品,探讨了脱除喹啉不溶物的操作条件,包括溶剂配比、沉降温度、沉降时间、减压蒸馏温度以及对不同原料制备的浸渍沥青产品性能比较,最后以曲靖中温沥青为原料制得了软化点83 ℃,喹啉不溶物0.084%,结焦值49.32%的浸渍剂沥青产品。

关键词: 煤沥青, 溶剂沉降法, 浸渍剂沥青

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