Progress in nanoparticles prepared by detonation method and their agglomeration control

doi:10.16085/j.issn.1000-6613.2020-0250

Abstract

Abstract:

Detonation method, which is regarded as a new method of preparing nanoparticles (NPs), has the advantages of simple operation, higher efficiency, lower cost, saving energy and environmental protection, etc. However, due to the complexity of the synthesis process and special properties of NPs, the explosive synthesis of NPs is easy to agglomerate, which not only destroys the ultra-fineness and uniformity of NPs, but also affects their superior performance. At present, the research on the NPs preparation by detonation method as well as their agglomeration control has been one of the hotspots in the field of explosive processing. In this study, research progress of NPs synthesized by detonation method is generalized. The latest achievements in controlling agglomeration of NPs and improving the dispersibility of NPs are summarized from the aspects of the main influencing factors, such as the physical and chemical properties of NPs, the preparation process, the purification process, the dispersion process, and the agglomeration models. The research hotspots and key problems, which needed to be solved urgently, are also presented.

Key words: nanoparticles, agglomerate structures, detonation method, dispersibility, synthetic process

摘要：

作为一种新兴的纳米材料制备方法，爆炸法具有操作简单、高效、经济、节能和环保等特点。但是，合成过程的复杂性和纳米材料特殊的性能，导致爆炸合成的纳米粉体极易团聚，这不仅破坏纳米粉体的超细性和均匀性，还影响其发挥自身的优越性能。目前，爆炸合成纳米粉体及其团聚控制研究已经成为爆炸加工领域的研究热点之一。本文首先概述了国内外爆炸合成纳米粉体的发展现状；然后从爆炸合成纳米粉体团聚的主要影响因素（如纳米粉体的理化特性、制备工艺、提纯工艺和分散工艺）和粉体团聚机理等方面综述了研究成果；最后指出了今后的研究热点和亟待解决的关键问题。

关键词: 纳米粉体, 团聚结构, 爆炸法, 分散性, 合成工艺

CLC Number:

O634.2

Yandong QU, Lingxia GAO, Wenjiao ZHANG, Wei LIU. Progress in nanoparticles prepared by detonation method and their agglomeration control[J]. Chemical Industry and Engineering Progress, 2020, 39(12): 5136-5147.

曲艳东, 高凌霞, 章文姣, 刘伟. 爆炸合成纳米粉体及其团聚控制研究进展[J]. 化工进展, 2020, 39(12): 5136-5147.

References

1	BAGGE-HANSEN M, BASTEA S, HAMMONS J A, et al. Detonation synthesis of carbon nano-onions via liquid carbon condensation [J]. Nature Communications, 2019, 10: 3819.
2	LI X J, QU Y D, XIE X H, et al. Preparation of SrAl₂O₄:Eu²⁺, Dy³⁺ nanometer phosphors by detonation method [J]. Materials Letters, 2006, 60(29): 3673–3677.
3	姜宗林, 滕宏辉, 刘云峰. 气相爆轰物理的若干研究进展[J]. 力学进展, 2012, 42(2): 129-140.
3	JIANG Zonglin, TENG Honghui, LIU Yunfeng. Some research progress on gaseous detonation physics [J]. Advances In Mechanics, 2012, 42(2): 129-140.
4	曲艳东, 孔祥清, 李晓杰, 等. 热处理对爆轰合成的纳米TiO₂混晶的结构相变的影响[J]. 物理学报, 2014, 63(3):037301.
4	QU Yandong, KONG Xiangqing, LI Xiaojie, et al. Effect of thermal treatment on the structural phase transformation of the detonation-prepared TiO₂ mixed crystal nanoparticles [J]. Acta Physica Sinica, 2014, 63(3): 037301.
5	曲艳东, 李晓杰, 刘元. 纳米氧化钛团聚结构的研究[J]. 高压物理学报, 2010, 24(6): 438-442.
5	QU Yandong, LI Xiaojie, LIU Yuan. Study on the agglomerate structures of TiO₂ nanoparticles [J]. Chinese Journal of High Pressure Physics, 2010, 24(6): 438-442.
6	HENSEL R C, MOREIRA M, RIUL A, et al. Monitoring the dispersion and agglomeration of silver nanoparticles in polymer thin films using localized surface plasmons and ferrell plasmons [J]. Applied Physics Letters, 2020, 116(10):103105.
7	TANG C, LI X, TANG Y, et al. Agglomeration mechanism and restraint measures of SiO₂nanoparticles in meta-aramid fibers doping modification via molecular dynamics simulations [J]. Nanotechnology, 2020, 31(16):165702.
8	李晓杰, 王旭光, 张勇, 等. 爆炸合成新材料中的几个关键问题[C]//王旭光. 爆炸合成新材料与高效、安全爆破关键技术科学和工程技术. 北京：冶金工业出版社, 2011.
8	LI Xiaojie, WANG Xuguang, ZHANG Yong, et al. Several key problems in explosive synthesis of new materials [C]//WANG Xuguang. Explosive synthetic new material and key technology of high efficiency and safety blasting science and engineering technology [M]. Beijing: Metallurgical Industry Press, 2011.
9	QU Y D, ZHANG W J, KONG X Q, et al. Theoretical investigation of calculating temperatures in the combining zone of Cu/Fe composite plate jointed by explosive welding [J]. Phys. Metals Metallogr., 2016, 117(3): 260–266.
10	KUZ'MIN E V, LYSAK V I, KUZ'MIN S V, et al. Effect of parameters of high-velocity collision on the structure and properties of joints upon explosive welding with simultaneous ultrasonication [J]. Phys. Metals Metallogr., 2019, 120(2): 197-203.
11	STEPAN S B, ALEXANDER N O, NAUMOV STEPAN P, et al. Novel synthesis and properties of hydrogen-free detonation nanodiamond [J]. Propell. Explos. Pyrot., 2015, 40(1):39-45.
12	KOMATSU T. Bulk synthesis and characterization of graphite-like B-C-N and B-C-N hetero diamond compounds [J]. J. Mater. Chem., 2004, 14(2): 221–227.
13	SIVKOV A A, NAIDEN E P, PAK A Y. Dynamic synthesis of ultradispersed crystalline phases of the C-N system[J]. J. Superhard Mater., 2009, 31(5): 300-305.
14	KOJIMA Y, OHFUJI H. Structure and stability of carbon nitride under high pressure and high temperature up to 125GPa and 3000K [J]. Diam. Relat. Mater., 2013, 39(10): 1–7.
15	WANG Y G, LIU F S, LIU Q J, et al. Recover of C₃N₄ nanoparticles under high-pressure by shock wave loading [J]. Ceram. Int., 2018, 44(16): 19290-19294.
16	LANGENDERFER M J, FAHRENHOLTZ W G, CHERTOPALOV S, et al. Detonation synthesis of silicon carbide nanoparticles [J]. Ceram. Int., 2020, 46(5): 6951-6954.
17	邵丙璜, 张晓堤. 爆炸合成纳米聚晶超硬材料及其制品的产业化前景[J]. 金刚石与磨料磨具工程, 2001(6):26-27.
17	SHAO Binghuang, ZHANG Xiaodi. Industrialization prospect of explosive synthesis of nano-polycrystalline superhard materials and its products [J]. Diamond and Abrasives Engineering, 2001(6):26-27.
18	TSVIGUNOV A N, FROLOVA L A, KHOTIN V G. Detonation synthesis of cuprite with a cubic face-centered lattice (a review) [J]. Glass & Ceramics, 2003, 60(9/10): 347-350.
19	李晓杰. 氧化物粉末的爆轰合成方法: CN1569617 [P]. 2005-01-26.
19	LI Xiaojie. Detonation synthesis of oxide powder: CN1569617 [P]. 2005-01-26.
20	QU Y D, LI X J, LI R Y, et al. Preparation and characterization of the TiO₂ ultrafine particles by detonation method [J]. Mater. Res. Bull., 2008, 43(1): 97-103.
21	LI R Y, LI X J, XIE X H. Explosive synthesis of ultrafine Al₂O₃ and effect of temperature of explosion [J]. Combust. Explos. Shock Waves, 2006, 42 (5): 607-610.
22	XIE X H, LI X J, YAN H H. Detonation synthesis of zinc oxide nanometer powders [J]. Mater. Lett., 2006, 60(25/26): 3149-3152.
23	李晓杰, 杜云艳, 王小红, 等. 爆轰法制备球形纳米CeO₂粉末[J].中国稀土学报, 2008, 26(2): 209-212.
23	LI Xiaojie, DU Yunyan, WANG Xiaohong, et al. Preparation of nanometer-sized ceria powders by detonation method [J]. Journal of the Chinese Rare Earth Society, 2008, 26(2): 209-212.
24	郑敏, 王作山. 爆炸法合成纳米α-Fe₂O₃[J]. 硅酸盐学报, 2005, 33(8):14-17.
24	ZHENG Min, WANG Zuoshan. Synthesis of α-Fe₂O₃ nanopowder by explosive method [J]. Journal of the Chinese Ceramic Society, 2005, 33(8): 14-17.
25	QU Y D, LI X J, YAN H H, et al. Selective synthesis of TiO₂ nanopowders [J]. Glass Phys. Chem., 2008, 34(5): 637–639.
26	解一超. 爆轰法制备纳米二氧化铈及其性能研究[D].南京:南京理工大学, 2013.
26	XIE Yichao. Study on preparation and properties of nano-cerium dioxide by detonation [D].Nanjing: Nanjing University of Science and Technology, 2013.
27	侯毅峰, 刘玉存, 王作山, 等. 爆炸法制备纳米氧化锆及其表征[J].含能材料, 2011, 19(1): 89–93.
27	HOU Yifeng, LIU Yucun, WANG Zuoshan, et al. Preparation and characterization of nanometer zirconia via explosive detonation technique[J]. Chinese Journal of Energetic Materials, 2011, 19(1): 89–93.
28	QU Y D, SUN C H, SUN G L, et al. Preparation, characterization, and kinetic and thermodynamic studies of mixed-phase TiO₂ nanoparticles prepared by detonation method [J]. Results in Physics, 2016, 6: 100–106.
29	VASYLKIV O, SAKKA Y, SKOROKHOD V V. Nano-explosion synthesis of multi-component ceramic nano-composites [J]. J. Eur. Ceram. Soc., 2007, 27 (2/3): 585–592.
30	WANG X H, LI X J, YAN H H, et al. Nano-MnFe₂O₄ powder synthesis by detonation of emulsion explosive [J]. Applied Physics A: Materials Science Processing, 2008, 90(3): 417-422.
31	QU Y D, LI X J, ZHAO Z, et al. Synthesis of SrAl₂O₄:Eu²⁺, Dy³⁺ nanometer phosphors by detonation and combustion method[J]. Chinese Journal of High Pressure Physics, 2008(2):175-180.
32	XIE X H, LI X J, ZHAO Z, et al. Growth and morphology of nanometer LiMn₂O₄ powder [J]. Powder Technology, 2006, 169(3):143-146.
33	LUO N, SUN X, LIANG H L, et al. Gas-liquid detonation synthesis of CNTs@Fe/Fe₃C composites and their application as electrode materials for double-layer capacitors[J]. Fuller. Nanotub. Carbon N., 2020, 28(6): 480-486.
34	冯余庆. 爆炸法合成钛酸锂材料的研究[D]. 淮南: 安徽理工大学, 2019.
34	FENG Yuqing. Study on synthesis of lithium titanate materials by explosion method [D]. Huainan:Anhui University of Technology, 2019.
35	WANG X H, GUO L, LI X J, et al. Controlled detonation synthesis of nano Fe-based oxides/SiO₂ core-shell composite particles[J]. Chemical Physics Letters, 2020, 740: 137016.
36	HAMMONS J A, NIELSEN M H, BAGGE-HANSEN M, et al. Resolving detonation nanodiamond size evolution and morphology at sub-microsecond timescales during high-explosive detonations[J]. J. Phys. Chem. C, 2019, 123(31): 19153-19164.
37	徐康, 薛群基. 炸药爆炸法合成的纳米金刚石粉[J]. 化学进展, 1997, 9(2): 201-208.
37	XU Kang, XUE Qunji. Nanometer-sized diamond powders synthesized by explosive detonation [J]. Progress in Chemistry, 1997, 9(2): 201-208.
38	文潮, 关锦清, 刘晓新, 等. 炸药爆轰合成纳米金刚石的研发历史与现状[J]. 超硬材料工程, 2009, 21(2): 46-51.
38	WEN Chao, GUAN Jinqing, LIU Xiaoxin, et al. Developing history and current situation of nano-diamond synthesized by explosive detonation[J]. Superhard Material Engineering, 2009, 21(2): 46-51.
39	苗卫朋, 丁玉龙, 翟黎鹏, 等.爆轰法合成纳米金刚石的分散技术研究进展[J].金刚石与磨料磨具工程, 2019, 39(1): 18-22.
39	MIAO Weipeng, DING Yulong, CUI Lipeng, et al. Progress of research on nano-diamond dispersion [J]. Diamond & Abrasives Engineering, 2019, 39(1): 18-22.
40	CHEN P W, HUANG F L, YUN S R. Optical characterization of nanocarbon phases in detonation soot and shocked graphite [J]. Diam. Relat. Mater., 2006, 15(9): 1400-1404.
41	SUN G L, LI X J, QU Y D, et al. Preparation and characterization of graphite nanosheets from detonation technique [J]. Mater. Lett., 2008, 62(4/5): 703-706.
42	LU Y, ZHU Z P, LIU Z Y. Catalytic growth of carbon nanotubes through CHNO explosive detonation [J]. Carbon, 2004, 42(2): 361-370.
43	ZOU Q, LI Y G, ZOU L H, et al. Characterization of structures and surface states of the nanodiamond synthesized by detonation [J]. Mater. Charact., 2009, 60(11): 1257-1262.
44	LUO N, XIANG J X, SHEN T, et al. One-step gas-liquid detonation synthesis of carbon nano-onions and their tribological performance as lubricant additives [J]. Diam. Relat. Mater. 2019, 97:107448.
45	PANICH AM, SHAMES AI, MOGILYANSKY D, et al. Detonation nanodiamonds fabricated from tetryl: synthesis, NMR, EPR and XRD study[J]. Diam. Relat. Mater., 2020, 108: 107918.
46	BUKAEMSKII A A, BELOSHAPKO A G. Explosive synthesis of ultradisperse aluminum oxide in an oxygen-containing medium [J]. Combust Explo. Shock Waves, 2001, 37(5): 594-599.
47	YAN H H, HUN C H, LI X J, et al. Synthesis of carbon-encapsulated iron nanoparticles by gaseous detonation of hydrogen and oxygen at different temperatures within detonation tube [J]. Rare Metal. Mat. Eng., 2015, 44(9): 2152-2155.
48	孔祥清，朱凯泽，高化东，等. 气相爆轰法制备纳米TiO₂-SiO₂复合氧化物及其表征[J]. 稀有金属与硬质合金， 2018, 46(1): 44-48.
48	KONG X Q, ZHU Z K, GAO H D, et al. Gaseous detonation synthesis and characterization of TiO₂-SiO₂ nanometer composite oxide[J]. Rare Metals and Cemented Carbides, 2018, 46(1): 44-48.
49	YAN Honghao, WU Linsong, LI Xiaojie, et al. Detonation synthesis of SnO₂ nanoparticles in gas phase [J]. Rare Metal. Mat. Eng., 2013, 42(7):1325-1327.
50	潘训岑, 李雪琪, 李晓杰, 等.气相爆轰法合成超细碳包铁纳米颗粒[J]. 稀有金属材料与工程, 2019, 48(3): 981-986.
50	PAN Xuncen, LI Xueqi, LI Xiaojie, et al. Research on synthesis of ultrafine carbon-encapsulated iron by gaseous detonation method [J]. Rare Metal. Mat. Eng., 2019, 48(3):981-986.
51	向俊庠, 罗宁, 马占国, 等. 爆炸合成石墨包覆金属(Fe, Co, Ni)纳米颗粒及其摩擦学性能[J]. 稀有金属材料与工程, 2019, 48(5):1682-1686.
51	XIANG Junxiang, LUO Ning, MA Zhanguo, et al. Explosive detonation synthesis and tribological performance of graphite coated metal nanoparticles [J]. Rare Metal. Mat. Eng., 2019, 48(5): 1682-1686.
52	TANAKA S, HOKAMOTO K, TORII S, et al. Surface coating by diamond particles on an aluminum substrate by underwater shock wave[J]. J. Mate. Process. Tech., 2010, 210(1): 32-36.
53	曲艳东, 孙从煌, 孔祥清, 等. 一种球形纳米混合氧化物(SiO-FeO)粉体的合成方法: CN105753069A[P]. 2016-07-13.
53	QU Yandong, SUN Conghuang, KONG Xiangqing, et al. A method to prepare spherical mixed oxide (SiO-FeO) nanoparticles: CN105753069A[P]. 2016-07-13.
54	ZHAO Tiejun, WANG Xiaohong, LI Xiaojie, et al. Gaseous detonation synthesis of Co@C nanoparticles/CNTs materials[J]. Mater. Lett., 2019, 236: 179-182.
55	LIU B Y, KE S Y, SHAO Y F, et al. Formation mechanism for oxidation synthesis of carbon nanomaterials and detonation process for core-shell structure [J]. Carbon, 2018, 127: 21-30.
56	JIANG T, XU K. FTIR study of ultradispersed diamond powder synthesized by explosive detonation [J]. Carbon, 1995, 33(12): 1663-1671.
57	JI S, JIANG T, XU K, et al. FTIR study of the adsorption of water on ultradispersed diamond powder surface [J]. Appl. Surf. Sci., 1998, 133(4): 231-238.
58	CHEN P W, DING Y S, CHEN Q, et al. Spherical nanometer-sized diamond obtained from detonation[J]. Diam. Relat. Mater.， 2000, 9(9):1722-1725.
59	XU K, XUE Q J. A new method for deaggregation of nanodiamond from explosive detonation-graphitization-oxidation method [J]. Acta Phys-Chim Sini, 2003, 19(11): 993-995.
60	YAMADA K, BURKHARD G, TANABE Y, et al. Nanostructure and formation mechanism of proto diamond shock-synthesized from graphite [J]. Carbon, 1999, 37(2): 275-280.
61	谢圣中. 爆轰纳米金刚石粒度分析研究[J]. 超硬材料工程, 2019, 31(4):18-21.
61	XIE Shengzhong. Analysis and research on the particle size of detonation nanodiamond [J]. Superhard Material Engineering, 2019, 31(4):18-21.
62	陈鹏万, 恽寿榕, 陈权, 等. 爆轰合成纳米超微金刚石的热稳定性研究[J]. 金刚石与磨料磨具工程, 1999(5): 3-5.
62	CHEN Pengwan, YUN Shourong, CHEN Quan, et al. The thermal stability of ultrafined diamond(UFD) obtained from detonation. [J]. Diamond & Abrasives Engineering, 1999(5): 3-5.
63	曲艳东, 孙从煌, 朱凯泽, 等.气相爆轰合成纳米TiO₂粉末的实验研究[J].稀有金属与硬质合金, 2017, 45(6): 48-53.
63	QU Yandong, SUN Conghuang, ZHU Kaize, et al. Experimental study on TiO₂ nanoparticles prepared by gaseous detonation [J]. Rare Metals and Cemented Carbides, 2017, 45(6): 48-53.
64	LI R Y, LI X J, YAN H H, et al. Experimental investigations of the controlled explosive synthesis of ultrafine Al₂O₃ [J]. Combust. Explo. Shock Waves, 2013, 49(1): 105-108.
65	KOLOMIICHUK V N, MAL'KOV I Y. Synthesis of an ultradispersed diamond phase during detonation of composites [J]. Combust. Explo. Shock Waves, 1993, 29(1): 113-112.
66	ANISICHKIN V F, DOLGUSHIN D S, PETROV E A. The effect of temperature on the growth of ultradispersed diamonds at a detonation front [J]. Combust. Explo. Shock Waves, 1995, 31(1): 106-109.
67	OUYANG X, LI X J, YAN H H, et al. Preparation and characterization of nanosized TiO₂ powders by gaseous detonation method [J]. Mater. Sci. Eng. B: Solid., 2008, 153(S1): 21-24.
68	韩志伟, 解立峰, 邓吉平, 等. 爆轰法合成纳米氧化铈粒径的控制[J].高压物理学报, 2014, 28(5): 585-590.
68	HAN Zhiwei, XIE Lifeng, DENG Jiping, et al. Size-control of nanostructured Ceria synthesized by detonation method [J]. Chinese Journal of High Pressure Physics, 2014, 28(5): 585-590.
69	闫鸿浩, 王胜杰, 李晓杰, 等. 氧气含量比变化对气相爆轰合成纳米二氧化钛的影响[J].材料工程, 2013, 25(6): 82-86.
69	YAN Honghao, WANG Shengjie, LI Xiaojie, et al. Influence of oxygen concentration on TiO₂ nanoparticles prepared by gaseous detonation [J]. Journal of Materials Engineering, 2013, 25(6): 82-86.
70	YAMADA K, SAWAOKA A B. Very small spherical crystals of distorted diamond found in a detonation product of explosive/graphite mixtures and their formation mechanism [J]. Carbon, 1994, 32(4): 665-673.
71	王小红, 李晓杰, 闫鸿浩, 等. 一类爆轰合成用乳化炸药的爆轰反应特征[J]. 爆炸与冲击, 2012, 32(5): 523-527.
71	WANG Xiaohong, LI Xiaojie, YAN Honghao, et al. Detonation reaction characteristic of emulsion explosives used for nano-materials synthesis [J]. Explosion and Shock Waves, 2012, 32(5): 523-527.
72	罗宁, 李晓杰, 王小红, 等. 硝酸铁对RDX热分解行为的影响[J].火工品, 2010(3): 39-43.
72	LUO Ning, LI Xiaojie, WANG Xiaohong, et al. Effect of ferric nitrate on thermal decomposition behavior of RDX [J]. Initiators & Pyrotechnics, 2010(3): 39-43.
73	张厚生, 胡荣祖, 杨德锁.多硝基芳香族化合物的分解热与爆热的关系[J].化学通报, 1987(12):30-32.
73	ZHANG Housheng, HU Rongzu, YANG Desuo. Relationship between the heat of decomposition and the heat of explosion of aromaticity [J] Chemistry, 1987(12):30-32.
74	WANG X H, LI X J, YAN H H, et al. Research of thermal decomposition kinetic characteristic of emulsion explosive base containing Fe and Mn elements[J]. J. Therm. Anal. Calorim., 2008, 91(2): 545-550.
75	QU Y D, LI X J, ZHAO Z, et al. Titania nanocrystalline prepared by detonation method and calculation of detonation parameters [J]. Propell. Explos. Pyrot., 2011, 36(1): 75-79.
76	PETROV E A, SAKOVICH G V, BRYLYAKOV P M. Conditions for preserving diamonds when produced by explosion [J]. Sov. Phys. Dokl., 1990, 35: 765-767.
77	SAVVAKIN G I, TREFILOV V I. Structure and properties of ultradisperse diamond formed during detonation in various media of condensed, carbon-containing explosives with negative oxygen balance [J]. Sov. Phys. Dokl., 1991, 36(11): 785-787.
78	MAL'KOV I Y, FILATOV L I, TITOV V M, et al. Formation of diamond from the liquid phase of carbon [J]. Combust. Explo. Shock Waves, 1993, 29(4): 542-544.
79	AMIN M H, MOTTALEBIZADEH A A, BORJI S. Influence of cooling medium on detonation synthesis of ultradispersed diamond [J]. Diam. Relat. Mater., 2009, 18(4): 611-614.
80	马峰, 恽寿榕, 陈权, 等. 装药及外界保护介质对炸药爆轰合成超微金刚石的影响[J].爆炸与冲击, 1998, 18(4): 289-295.
80	MA Feng, YUN Shourong, CHEN Quan, et al. The influence of charge and preserving media on the yield of ultrafine diamond formation during detonation [J]. Explosion and Shock Waves, 1998, 18(4): 289-295.
81	王志伟, 李艳国, 邹芹, 等. 后处理对爆轰纳米金刚石表面官能团的影响[J].矿冶工程, 2020, 40(1):125-129.
81	WANG Zhiwei, LI Yanguo, ZOU Qin, et al. Effect of post-treatment on surface functional groups of detonation nanodiamonds[J]. Mining and Metallurgical Engineering, 2020, 40(1):125-129.
82	DONNET J B, FOUSSON E, WANG T K, et al. Dynamic synthesis of diamonds [J]. Diam. Relat. Mater., 2000, 9(S3/S4/S5/S6): 887-892.
83	OKOTRUB A V, BULUSHEVA L G, LARIONOVA I S, et al. Surface electronic structure of detonation nanodiamonds after oxidative treatment [J]. Diam. Relat. Mater., 2007, 16(12): 2090-2092.
84	HA S, HONG S P, LEE M, et al. Chemical purification of detonation-synthesized nanodiamond: recycling of H₂SO₄ and optimization of process parameters [J]. Materials Today Communications, 2019, 21: 100571.
85	QU Y D, LI X J, WANG X H, et al. Detonation synthesis of nanosized titanium dioxide powders [J]. Nanotechnology, 2007, 18: 205602.
86	PICHOT V, COMET M, FOUSSON E, et al. An efficient purification method for detonation nanodiamonds [J]. Diam. Rel. Mater., 2008, 17(1): 13-22.
87	SHENDEROVA O, PETROV I, WALSH J, et al. Modification of detonation nanodiamonds by heat treatment in air [J]. Diam. Rel. Mater, 2006, 15(S11/S12): 1799-1803.
88	ACKERMANNA J, KRUEGER A. Efficient surface functionalization of detonation nanodiamond using ozone under ambient conditions [J]. Nanoscale, 2019, 11: 8012-8019.
89	KUME A, MOCHALIN V N. Sonication-assisted hydrolysis of ozone oxidized detonation nanodiamond [J]. Diam. Relat. Mater., 2020,103:107705.
90	XU K, XUE Q. A new method for deaggregation of nanodiamond from explosive detonation: graphitization-oxidation method [J]. Phys. Solid. State., 2003, 46(4): 649-650.
91	LI X J, QU Y D, YAN H H, et al. Research progress on nanosized materials synthesized by detonation method [J]. Rare Metal. Mat. Eng., 2007, 36(12): 2069-2074.
92	QU Y D, LI X J, YAN H H. Heat transfer analysis of the micron-scale agglomerates of TiO₂ precursor during the detonation process [J]. Adv. Mater. Res., 2011, 306/307: 1138-1141.
93	许向阳. 纳米金刚石的解团聚与稳定分散研究[D]. 长沙: 中南大学, 2007.
93	XU Xiangyang. Deagglomeration and stable dispersion of detonation nanodiamond particles[D].Changsha: Central South University, 2007.
94	TSE J S, KLUG D, GAO F. Hardness of nanocrystalline diamonds [J]. Phys. Rev. B, 2006, 73(14): 140102.
95	KRüGER A, LIANG Y J, JARRE G, et al. Surface functionalisation of detonation diamond suitable for biological applications [J]. J. Mater. Chem., 2006, 16(24): 2322-2328.
96	李晓杰, 易彩虹, 王小红, 等. 爆轰纳米金刚石在水中稳定分散研究[J]. 材料科学与工艺, 2011, 19(5): 144-148.
96	LI Xiaojie, YI Caihong, WANG Xiaohong, et al. Stable dispersion of detonation nanodiamond in aqueous medium [J]. Mater. Sci. Tech., 2011,19(5): 144-148.
97	LI C C, HUANG C L. Preparation of clear colloidal solutions of detonation nanodiamond in organic solvents [J]. Colloids Surf. A, 2010, 353(1): 52-56.
98	ZHU Y, XU X, WANG B, et al. Surface modification and dispersion of nanodiamond in clean oil [J]. China Particuology, 2004, 2(3): 132-134.
99	MITEV D P, TOWNSEND A T, PAULL B, et al. Microwave-assisted purification of detonation nanodiamond [J]. Diam. Relat. Mater., 2014, 48: 37-46.
100	BERGMANN O R, BARRINGTON J. Effect of explosive shock waves on ceramic powders [J]. J. Am. Ceram. Soc., 1966, 49(9): 502-507.
101	薛鸿陆, 洪延姬. 冲击波对氮化铝粉体的活化及烧结[J].爆炸与冲击, 1995, 15 (4): 322-328.
101	XUE Honglu, HONG Yanji. Aluminum nitride activated and sintered under shock pressure [J]. Explosion and Shock Waves, 1995, 15 (4):322-328.
102	钟盛文, 焦永斌, 匡敬忠. 爆炸冲击粉碎纳米粉末硬团聚体的机理分析[J].中国粉体技术, 2000(5): 19-22.
102	ZHONG Shenwen, JIAO Yongbin, KUANG Jingzhong. Mechanism analysis of impact crushing of harden nano aggregation powder by shock wave [J]. China Powder Science and Technology, 2000(5): 19-22.
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