Research progress on flow regimes and mass transfer of liquid-liquid two-phase flow in microchannels

doi:10.16085/j.issn.1000-6613.2018-0826

Abstract

Abstract:

Liquid-liquid two-phase flow in microchannels plays an important role in micro-chemical engineering. Understanding the role of liquid-liquid two-phase flow, mixing and mass transfer in microchannels is of great importance for improving its industrial applications. This paper mainly focused on the liquid-liquid two-phase flow in microchannels, summarized the different flow patterns and mass transfer coefficients of the liquid-liquid two-phase flow under different operating conditions. The influence of various factors including features of microchannels, properties and flow rates of fluids on the formation of flow patterns and mass transfer coefficients were analyzed. It was pointed out that most of researches on liquid-liquid two-phase flow in microchannels were qualitative. Quantitative researches were aimed at the specific systems and the results haven a few limitations. Moreover, researches on mass transfer of liquid-liquid two-phase flow in microchannels are conducted experimentally and there are relatively few numerical simulations. Thus, the following studies should be considered to establish the database based on the fundamental researches of liquid-liquid two-phase flow. Based on the analysis of numerous data the criteria of regime classification and empirical formulas should be gained for improving its industrial applications. The numerical simulation models were deserved to develop the effective evaluation mechanisms on mass transfer efficiency in liquid-liquid two-phase flow.

Key words: liquid- liquid two-phase flow, flow regimes, mixing and mass transfer, microchannels

摘要：

微通道内液-液两相流流动在微化工系统中占有重要的地位，了解微通道内液-液两相流体流动和传质规律对推动其工业化应用有重要作用。本文以微通道内液-液两相流系统为研究对象，简述了不同工况下微通道内液-液两相流流型和混合传质效率，分析了微通道特征、流体性质和流体流动速度等对流型形成和传质效率的影响。指出目前对于微通道内液-液两相流的研究多处于定性研究，定量研究仅针对某一体系展开，所得结果具有一定的局限性。关于微通道内液-液两相流传质研究实验较多而数值模拟方法相对较少，接下来的研究工作中应该考虑建立微通道内液-液两相流基础研究的数据库，通过分析大量的数据获得有效的流型划分准则和相关经验式以此推动微通道内液-液两相流的工业化应用。同时在传质研究过程中应研究开发相应的数值模拟模型，保证实验和数值模拟相结合，提出有效的传质效率评价机制。

关键词: 液-液两相流, 流型, 混合传质, 微通道

CLC Number:

TQ051.5

Jinyuan QIAN, Xiaojuan LI, Zan WU, Minrui CHEN, Zhijiang JIN, Bengt SUNDÉN. Research progress on flow regimes and mass transfer of liquid-liquid two-phase flow in microchannels[J]. Chemical Industry and Engineering Progress, 2019, 38(04): 1624-1633.

钱锦远, 李晓娟, 吴赞, 陈珉芮, 金志江, 蒙特桑顿. 微通道内液-液两相流流型及传质的研究进展[J]. 化工进展, 2019, 38(04): 1624-1633.

Figures/Tables 7

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参考文献	微通道材料、入口结构、尺寸/μm	两相体系、流动工况	变量	流型
[8]	石英、玻璃，双T型，d _h=793、667	水-矿物油 u _c=0～40cm·s^?1，u _d=0～20cm·s^?1	两相流速	弹状流、滴状流、分层流、半分层流
[9]	十字交叉型	硅油-不同浓度乙醇溶液 u _c=0.001～1.0m·s^?1， u _d=0.001～1.0m·s^?1	两相流速、表面张力、连续相黏度、壁面接触角	弹状流、滴状流、喷射流、节状形变流、管状流、滑移流
[10]	聚甲基丙烯酸甲酯（PMMA），T型共流，h×w=600×300	水-煤油 u _c=9.26×10^-4～1.85m·s^?1， u _d=9.26×10^-4～2.78m·s^?1	韦伯数	弹状流、滴状流、液滴群流、波平行流、平行流、混乱的细条纹流
[12]	聚全氟乙丙烯（FEP）、四氟乙烯（Tefzel）、玻璃，T型-圆截面，d _h=200、270	离子液体-水 Q _total=0.065～214.9cm³·h^?1， Q _IL/(Q _IL+Q _w)=0.05～0.8	壁面润湿性、总流速、流量比	弹状流、滴状流、节状形变流、弹状-滴状流、雾状流、不规则流
[14]	玻璃，Y型，d _h=260、760	正丁醇-水、乙酸正丁酯-水、甲苯-水	两相流速、通道尺寸、表面张力、壁面润湿性	弹状流、液滴流、弹状-液滴流、平行流
[24]	聚四氟乙烯（PTFE），Y型，d _h=250～1000	环己烷-水 Q _c=5～200mL·h^?1，Q _d=5～200mL·h^?1	微通道尺寸、两相流量	弹状流、滴状流、变形界面流
[25]	玻璃，十字交叉型，T型共流，h×w=200×200、400×400、600×600、300×600	水-丁醇、水-乙烷、水-甲苯、水-油	通道尺寸、两相黏度、表面张力	弹状流、滴状流、环状流
[26]	聚甲基丙烯酸甲酯（PMMA）,T型错流，h×w=150×200	u _c=0.001～0.1m·s^?1， u _d=0.001～0.1m·s^?1，Ca _c=10^-4～0.3	毛细数	弹状流、过渡流、滴状流
[27]	聚二甲基硅氧烷（PDMS），T型错流，h×w=80×100	硅油-甘油溶液 Q _c=2.4～100mL·h^?1， Q _d=2mL·h^?1、8mL·h^?1	连续相流量	弹状流
[28]	聚二甲基硅氧烷（PDMS）,Y型, w _c×w _d×h×α=100×200×100×80°、100×200×50×80°、170×170×80×60°	Q _c=2～120μL·min^?1， Q _d=2～120μL·min^?1	微通道几何尺寸	弹状流、滴状流、分层流
[29]	聚二甲基硅氧烷（PDMS），T型错流，d _h=400、600	水-植物油 Q _c=0.1～6mL·h^?1，Q _d=0.1～6mL·h^?1	两相流量、通道直径	弹状流
[30]	聚甲基丙烯酸甲酯（PMMA），T型错流，h×w=400×400、400×600、400×800	水与甘油的混合液-环己烷 Q _c=0～200mL·h^?1，Q _d=10～25mL·h^?1	两相流率、连续相黏度、毛细数、微通道尺寸	弹状流、过渡流、滴状流
[31]	聚二甲基硅氧烷（PDMS），Y型， α= 45°、90°、135°、180°，h×w=500×500	无水乙醇-液体石蜡 Ca _c=0.016、0.213、0.267， Ca _d=0.004、0.0027	Y型角度、毛细数	弹状流、液滴流、喷射流、平行流
[32]	聚二甲基硅氧烷（PDMS），双T型， d _h=176，h/w=2.4	硅油-水	两相流量	滴状流、弹状流、波平行流、平行流
[33]	玻璃，十字交叉型，h×w=200×200、400×400、600×600	水-丁醇、水-乙烷、水-甲苯、水-油、水/甘油（质量比60∶40）-油	通道尺寸、两相流速、两相黏度、表面张力	管状流、滴状流、喷射流

参考文献	微通道材料、入口结构、尺寸/μm	两相体系、流动工况	变量	流型
[8]	石英、玻璃，双T型，d _h=793、667	水-矿物油 u _c=0～40cm·s^?1，u _d=0～20cm·s^?1	两相流速	弹状流、滴状流、分层流、半分层流
[9]	十字交叉型	硅油-不同浓度乙醇溶液 u _c=0.001～1.0m·s^?1， u _d=0.001～1.0m·s^?1	两相流速、表面张力、连续相黏度、壁面接触角	弹状流、滴状流、喷射流、节状形变流、管状流、滑移流
[10]	聚甲基丙烯酸甲酯（PMMA），T型共流，h×w=600×300	水-煤油 u _c=9.26×10^-4～1.85m·s^?1， u _d=9.26×10^-4～2.78m·s^?1	韦伯数	弹状流、滴状流、液滴群流、波平行流、平行流、混乱的细条纹流
[12]	聚全氟乙丙烯（FEP）、四氟乙烯（Tefzel）、玻璃，T型-圆截面，d _h=200、270	离子液体-水 Q _total=0.065～214.9cm³·h^?1， Q _IL/(Q _IL+Q _w)=0.05～0.8	壁面润湿性、总流速、流量比	弹状流、滴状流、节状形变流、弹状-滴状流、雾状流、不规则流
[14]	玻璃，Y型，d _h=260、760	正丁醇-水、乙酸正丁酯-水、甲苯-水	两相流速、通道尺寸、表面张力、壁面润湿性	弹状流、液滴流、弹状-液滴流、平行流
[24]	聚四氟乙烯（PTFE），Y型，d _h=250～1000	环己烷-水 Q _c=5～200mL·h^?1，Q _d=5～200mL·h^?1	微通道尺寸、两相流量	弹状流、滴状流、变形界面流
[25]	玻璃，十字交叉型，T型共流，h×w=200×200、400×400、600×600、300×600	水-丁醇、水-乙烷、水-甲苯、水-油	通道尺寸、两相黏度、表面张力	弹状流、滴状流、环状流
[26]	聚甲基丙烯酸甲酯（PMMA）,T型错流，h×w=150×200	u _c=0.001～0.1m·s^?1， u _d=0.001～0.1m·s^?1，Ca _c=10^-4～0.3	毛细数	弹状流、过渡流、滴状流
[27]	聚二甲基硅氧烷（PDMS），T型错流，h×w=80×100	硅油-甘油溶液 Q _c=2.4～100mL·h^?1， Q _d=2mL·h^?1、8mL·h^?1	连续相流量	弹状流
[28]	聚二甲基硅氧烷（PDMS）,Y型, w _c×w _d×h×α=100×200×100×80°、100×200×50×80°、170×170×80×60°	Q _c=2～120μL·min^?1， Q _d=2～120μL·min^?1	微通道几何尺寸	弹状流、滴状流、分层流
[29]	聚二甲基硅氧烷（PDMS），T型错流，d _h=400、600	水-植物油 Q _c=0.1～6mL·h^?1，Q _d=0.1～6mL·h^?1	两相流量、通道直径	弹状流
[30]	聚甲基丙烯酸甲酯（PMMA），T型错流，h×w=400×400、400×600、400×800	水与甘油的混合液-环己烷 Q _c=0～200mL·h^?1，Q _d=10～25mL·h^?1	两相流率、连续相黏度、毛细数、微通道尺寸	弹状流、过渡流、滴状流
[31]	聚二甲基硅氧烷（PDMS），Y型， α= 45°、90°、135°、180°，h×w=500×500	无水乙醇-液体石蜡 Ca _c=0.016、0.213、0.267， Ca _d=0.004、0.0027	Y型角度、毛细数	弹状流、液滴流、喷射流、平行流
[32]	聚二甲基硅氧烷（PDMS），双T型， d _h=176，h/w=2.4	硅油-水	两相流量	滴状流、弹状流、波平行流、平行流
[33]	玻璃，十字交叉型，h×w=200×200、400×400、600×600	水-丁醇、水-乙烷、水-甲苯、水-油、水/甘油（质量比60∶40）-油	通道尺寸、两相流速、两相黏度、表面张力	管状流、滴状流、喷射流

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