Abstract: The effects of activated carbon，Ni and Pd/C catalysts on the hydrogenation of Shenfu coal were examined by using methanol as the solvent for both reaction and extraction under mild reaction conditions (140 ℃，initial hydrogen pressure 0.7 MPa，microwave irradiation 15 min). The results showed that the solubility of Shenfu coal in methanol increased in the order: non-catalytic hydrogenation

摘要： 以甲醇作为溶剂和萃取剂考察了在较温和的条件（140 oC，氢气初压0.7 MPa，微波辐射15 min）下活性炭、Ni和Pd/C催化剂对神府煤加氢反应的影响。结果表明：反应混合物在甲醇中的萃取率按非催化加氢< AC催化的加氢< Ni催化的加氢< Pd/C催化的加氢的顺序递增；通过GC/MS和FTIR分析可看出在不同反应条件下萃取物和萃余物组成的变化。