Chemical Industry and Engineering Progress ›› 2021, Vol. 40 ›› Issue (3): 1438-1448.DOI: 10.16085/j.issn.1000-6613.2020-0915
• Industrial catalysis • Previous Articles Next Articles
ZHAO Zhaoyang(), LUO Xiaoyan, PEI Baoyou, XIANG Xiaoyan, LI Jiaran, MA Ruixun, ZHANG Ziheng, LIN Jinqing()
Received:
2020-05-25
Online:
2021-03-17
Published:
2021-03-05
Contact:
LIN Jinqing
赵朝阳(), 罗小燕, 裴宝有, 项小燕, 李佳然, 马瑞勋, 张子姮, 林金清()
通讯作者:
林金清
作者简介:
赵朝阳(1995—),男,硕士研究生,研究方向为离子液体及绿色催化。E-mail:基金资助:
CLC Number:
ZHAO Zhaoyang, LUO Xiaoyan, PEI Baoyou, XIANG Xiaoyan, LI Jiaran, MA Ruixun, ZHANG Ziheng, LIN Jinqing. Research progress on CO2 cycloaddition catalyzed by porous hyper-crosslinked polymers immobilized ionic liquids[J]. Chemical Industry and Engineering Progress, 2021, 40(3): 1438-1448.
赵朝阳, 罗小燕, 裴宝有, 项小燕, 李佳然, 马瑞勋, 张子姮, 林金清. 多孔超交联聚合物固载离子液体催化二氧化碳环加成反应的研究进展[J]. 化工进展, 2021, 40(3): 1438-1448.
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催化剂 | 单体 | 底物 | 压力 /MPa | 温度 /℃ | 时间 /h | 产率 /% | 参考文献 |
---|---|---|---|---|---|---|---|
AIMDFP | 双氰胺 | 环氧丙烷 | 2 | 130 | 3.5 | 99 | [ |
P(DMAEMA-EtOH)Br | 甲基丙烯酸二甲氨基乙酯 | 环氧丙烷 | 2 | 110 | 3 | 96.2 | [ |
PDMBr | 1-乙烯基咪唑 | 环氧丙基苯基醚 | 0.1 | 70 | 48 | 90 | [ |
PIP-Bn-Cl | 乙烯基功能化的三苯基膦 | 环氧丙烷 | 0.1 | 50 | 24 | 93.2 | [ |
Polymer 1 | 三苯基膦 | 氧化苯乙烯 | 1 | 130 | 12 | 96 | [ |
PVIm-6-SCD | 1-乙烯基咪唑1,2,3,4,5,6-六苄溴苯 | 环氧丙烷 | 0.1 | 50 | 24 | 99.5 | [ |
DVB@ISA | 1-乙烯基咪唑二乙烯基苯1,2-环己二胺 | 1,2-环氧己烷 | 1 | 60 | 24 | 99 | [ |
AE-PIL-Cl | 1-乙烯基咪唑乙烯基苯 | 环氧丙烷 | 1 | 140 | 60 | 99 | [ |
1P+Br-&1PPh3@POPs | 乙烯基功能化的三苯基膦 | 环氧丙烷 | 3 | 120 | 5 | 90 | [ |
IHCP-OH(1) | 二乙烯基苯 1-乙烯基咪唑等 | 环氧丙基苯基醚 | 1 | 120 | 2 | 90 | [ |
[AlTMG]Br | 乙烯基苯功能化的季铵离子液体 | 环氧苯乙烯 | 0.1 | 100 | 6 | 99 | [ |
[PAD][IDA] | 二乙烯基苯 1-乙烯基咪唑 | 环氧苯乙烯 | 0.1 | 65 | 12 | 99 | [ |
Py-Im-6 | 1-乙烯基咪唑1,2,3,4,5,6-六苄溴 | 环氧丙烷 | 0.1 | 120 | 1 | 94.5 | [ |
PIL-4 | 1-乙烯基咪唑二(2-氯乙基)醚 | 环氧氯丙烷 | 1 | 100 | 12 | 99 | [ |
NHC-CAP-1(Zn2+) | 苯基咪唑等 | 环氧氯丙烷 | 2 | 100 | 3 | 97 | [ |
IC2HCP-5b | 1-苄基咪唑等 | 环氧氯丙烷 | 3 | 120 | 20 | 99 | [ |
IM-iPHP-2 | 1-苄基咪唑VPSOSS | 环氧氯丙烷 | 0.1 | 80 | 48 | 99 | [ |
V-iPHP-1 | 4,4-联吡啶等 | 环氧氯丙烷 | 0.1 | 60 | 72 | 99 | [ |
T-IM | 含咪唑的交联单体等 | 环氧氯丙烷 | 1 | 140 | 10 | 87(1H NMR) | [ |
PP-Br | 三(4-氯苯基)膦 | 环氧丙基苯基醚 | 0.1 | 140 | 20 | 98.5 | [ |
CPP-IL | 1,2-二甲基-3-(丙-2-炔基)-1H-咪唑-3-溴化铵等 | 环氧氯丙烷 | 0.1 | 100 | 24 | 99 | [ |
PAM-PyMe(Cl) | 2,6-二氨基吡啶 | 环氧氯丙烷 | 0.1 | 100 | 20 | 77 | [ |
UIIP | 含有咪唑的交联单体 | 环氧丙烷 | 1 | 110 | 2 | 97 | [ |
HIP-Br-2 | 苯基咪唑等 | 环氧丙烷 | 0.1 | 55 | 96 | 99 | [ |
HPILs-Cl | 苯基咪唑等 | 环氧丙烷 | 0.1 | 70 | 9 | 99(1H NMR) | [ |
IMIN-Br-OH | 咪唑修饰的四苯甲烷 | 环氧氯丙烷 | 0.1 | 40 | 72 | 99(1H NMR) | [ |
HMIB | 1,4-对二氯苄咪唑 | 环氧丙烷 | 1 | 110 | 1.5 | 90 | [ |
COP-222 | 对苯二甲醛氯化铵 | 环氧氯丙烷 | 0.1 | 100 | 24 | 99(1H NMR) | [ |
POM3-IM | 1-甲基咪唑等 | 环氧丙烷 | 1 | 120 | 4 | 78 | [ |
PS-[CETBD]Br | 氯球(PS-Cl) | 环氧丙烷 | 2 | 140 | 2 | 96.3 | [ |
PQA-NH2Py-Br | 2-氨基吡啶 | 1-丁基-2-苯基氮丙啶 | 2 | 70 | 4 | 99(1H NMR) | [ |
催化剂 7 | 4-乙烯基吡啶 | 环氧丙基苯醚 | 0.1 | 80 | 12 | 66(1H NMR) | [ |
催化剂 | 单体 | 底物 | 压力 /MPa | 温度 /℃ | 时间 /h | 产率 /% | 参考文献 |
---|---|---|---|---|---|---|---|
AIMDFP | 双氰胺 | 环氧丙烷 | 2 | 130 | 3.5 | 99 | [ |
P(DMAEMA-EtOH)Br | 甲基丙烯酸二甲氨基乙酯 | 环氧丙烷 | 2 | 110 | 3 | 96.2 | [ |
PDMBr | 1-乙烯基咪唑 | 环氧丙基苯基醚 | 0.1 | 70 | 48 | 90 | [ |
PIP-Bn-Cl | 乙烯基功能化的三苯基膦 | 环氧丙烷 | 0.1 | 50 | 24 | 93.2 | [ |
Polymer 1 | 三苯基膦 | 氧化苯乙烯 | 1 | 130 | 12 | 96 | [ |
PVIm-6-SCD | 1-乙烯基咪唑1,2,3,4,5,6-六苄溴苯 | 环氧丙烷 | 0.1 | 50 | 24 | 99.5 | [ |
DVB@ISA | 1-乙烯基咪唑二乙烯基苯1,2-环己二胺 | 1,2-环氧己烷 | 1 | 60 | 24 | 99 | [ |
AE-PIL-Cl | 1-乙烯基咪唑乙烯基苯 | 环氧丙烷 | 1 | 140 | 60 | 99 | [ |
1P+Br-&1PPh3@POPs | 乙烯基功能化的三苯基膦 | 环氧丙烷 | 3 | 120 | 5 | 90 | [ |
IHCP-OH(1) | 二乙烯基苯 1-乙烯基咪唑等 | 环氧丙基苯基醚 | 1 | 120 | 2 | 90 | [ |
[AlTMG]Br | 乙烯基苯功能化的季铵离子液体 | 环氧苯乙烯 | 0.1 | 100 | 6 | 99 | [ |
[PAD][IDA] | 二乙烯基苯 1-乙烯基咪唑 | 环氧苯乙烯 | 0.1 | 65 | 12 | 99 | [ |
Py-Im-6 | 1-乙烯基咪唑1,2,3,4,5,6-六苄溴 | 环氧丙烷 | 0.1 | 120 | 1 | 94.5 | [ |
PIL-4 | 1-乙烯基咪唑二(2-氯乙基)醚 | 环氧氯丙烷 | 1 | 100 | 12 | 99 | [ |
NHC-CAP-1(Zn2+) | 苯基咪唑等 | 环氧氯丙烷 | 2 | 100 | 3 | 97 | [ |
IC2HCP-5b | 1-苄基咪唑等 | 环氧氯丙烷 | 3 | 120 | 20 | 99 | [ |
IM-iPHP-2 | 1-苄基咪唑VPSOSS | 环氧氯丙烷 | 0.1 | 80 | 48 | 99 | [ |
V-iPHP-1 | 4,4-联吡啶等 | 环氧氯丙烷 | 0.1 | 60 | 72 | 99 | [ |
T-IM | 含咪唑的交联单体等 | 环氧氯丙烷 | 1 | 140 | 10 | 87(1H NMR) | [ |
PP-Br | 三(4-氯苯基)膦 | 环氧丙基苯基醚 | 0.1 | 140 | 20 | 98.5 | [ |
CPP-IL | 1,2-二甲基-3-(丙-2-炔基)-1H-咪唑-3-溴化铵等 | 环氧氯丙烷 | 0.1 | 100 | 24 | 99 | [ |
PAM-PyMe(Cl) | 2,6-二氨基吡啶 | 环氧氯丙烷 | 0.1 | 100 | 20 | 77 | [ |
UIIP | 含有咪唑的交联单体 | 环氧丙烷 | 1 | 110 | 2 | 97 | [ |
HIP-Br-2 | 苯基咪唑等 | 环氧丙烷 | 0.1 | 55 | 96 | 99 | [ |
HPILs-Cl | 苯基咪唑等 | 环氧丙烷 | 0.1 | 70 | 9 | 99(1H NMR) | [ |
IMIN-Br-OH | 咪唑修饰的四苯甲烷 | 环氧氯丙烷 | 0.1 | 40 | 72 | 99(1H NMR) | [ |
HMIB | 1,4-对二氯苄咪唑 | 环氧丙烷 | 1 | 110 | 1.5 | 90 | [ |
COP-222 | 对苯二甲醛氯化铵 | 环氧氯丙烷 | 0.1 | 100 | 24 | 99(1H NMR) | [ |
POM3-IM | 1-甲基咪唑等 | 环氧丙烷 | 1 | 120 | 4 | 78 | [ |
PS-[CETBD]Br | 氯球(PS-Cl) | 环氧丙烷 | 2 | 140 | 2 | 96.3 | [ |
PQA-NH2Py-Br | 2-氨基吡啶 | 1-丁基-2-苯基氮丙啶 | 2 | 70 | 4 | 99(1H NMR) | [ |
催化剂 7 | 4-乙烯基吡啶 | 环氧丙基苯醚 | 0.1 | 80 | 12 | 66(1H NMR) | [ |
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